采用高效液相色谱法测定黄连中盐酸小檗碱的含量
채용고효액상색보법측정황련중염산소벽감적함량
Determination of Berberine hydrochloride in Coptis by High Performance Liquid Chromatography
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    贵阳中医学院学报 귀양중의학원학보
    JOURNAL OF GUIYANG COLLEGE OF TRADITIONAL CHINESE MEDICINE
    2010年 5期 14-16 ,共3页

    苏松柏%张永萍

    소송백%장영평

    黄连%盐酸小檗碱%HPLC 黃連%鹽痠小檗堿%HPLC
    황련%염산소벽감%HPLC
    目的:采用高效液相色谱法(HPLC)测定黄连中盐酸小檗碱含量.方法:用C18色谱柱,以乙腈-0.1%磷酸水溶液(48:52),每100mL加入十二烷基磺酸钠0.1g为流动相,于265nm处测定.结果:盐酸小檗碱平均回收率为102.7%.结论:此法简便快速,准确稳定,重现性好,成本低.
    목적:채용고효액상색보법(HPLC)측정황련중염산소벽감함량.방법:용C18색보주,이을정-0.1%린산수용액(48:52),매100mL가입십이완기광산납0.1g위류동상,우265nm처측정.결과:염산소벽감평균회수솔위102.7%.결론:차법간편쾌속,준학은정,중현성호,성본저.
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