CAJ | 학술논문

目的:测定复方氯霉素洗剂及氯霉素地塞米松磷酸钠滴耳液中二组份的含量.方法:采用新Vierordt法不经分离直接测定复方氯霉素洗剂及氯霉素地塞米松磷酸钠滴耳液中氯霉素、水杨酸及地塞米松磷酸钠、氯霉素的含量.结果:以278,302nm分别为复方氯霉素洗剂中两组分的测定波长,以无水乙醇为空白,氯霉素和水杨酸的平均回收率及RSD分别为100.32%,0.16%和99.95%,0.23%;以242,278nm为氯霉素地塞米松磷酸钠滴耳液中两组份的测定波长,以蒸馏水为空白,地塞米松磷酸钠和氯霉素的平均回收率及RSD分别为99.86%,1.39%和100.28%,0.13%.结论:本法操作简便快速,重现性好,可消除各处方中二组份的相互干扰,结果满意.
목적:측정복방록매소세제급록매소지새미송린산납적이액중이조빈적함량.방법:채용신Vierordt법불경분리직접측정복방록매소세제급록매소지새미송린산납적이액중록매소、수양산급지새미송린산납、록매소적함량.결과:이278,302nm분별위복방록매소세제중량조분적측정파장,이무수을순위공백,록매소화수양산적평균회수솔급RSD분별위100.32%,0.16%화99.95%,0.23%;이242,278nm위록매소지새미송린산납적이액중량조빈적측정파장,이증류수위공백,지새미송린산납화록매소적평균회수솔급RSD분별위99.86%,1.39%화100.28%,0.13%.결론:본법조작간편쾌속,중현성호,가소제각처방중이조빈적상호간우,결과만의.