材料工程
材料工程
재료공정
JOURNAL OF MATERIALS ENGINEERING
2010年
3期
18-21
,共4页
姜大川%谭毅%董伟%王强%彭旭%李国斌
薑大川%譚毅%董偉%王彊%彭旭%李國斌
강대천%담의%동위%왕강%팽욱%리국빈
电子束%冶金硅%去除磷
電子束%冶金硅%去除燐
전자속%야금규%거제린
electron beam%metallurgical grade silicon%dephosphorization
采用电子束设备对多晶硅进行熔炼,设计熔炼功率和时间相同、降束时间不同的三组实验,评价硅中杂质磷在熔炼及凝固过程中的去除效果.根据熔炼后硅锭的杂质分布特点推导出表征硅中杂质磷的去除率公式,经计算得到去除率为80%以上,并由磷的蒸发方程计算出在本实验中当电子束熔炼多晶硅锭的束流密度在235mA之上时,硅中的磷都可以被蒸发去除.
採用電子束設備對多晶硅進行鎔煉,設計鎔煉功率和時間相同、降束時間不同的三組實驗,評價硅中雜質燐在鎔煉及凝固過程中的去除效果.根據鎔煉後硅錠的雜質分佈特點推導齣錶徵硅中雜質燐的去除率公式,經計算得到去除率為80%以上,併由燐的蒸髮方程計算齣在本實驗中噹電子束鎔煉多晶硅錠的束流密度在235mA之上時,硅中的燐都可以被蒸髮去除.
채용전자속설비대다정규진행용련,설계용련공솔화시간상동、강속시간불동적삼조실험,평개규중잡질린재용련급응고과정중적거제효과.근거용련후규정적잡질분포특점추도출표정규중잡질린적거제솔공식,경계산득도거제솔위80%이상,병유린적증발방정계산출재본실험중당전자속용련다정규정적속류밀도재235mA지상시,규중적린도가이피증발거제.
In order to evaluate the effect of dephosphorization in silicon during melting and solidification,three-group electron beam melting experiments with the same melting power but different time for extinguishing beam density were carried out. According to the distribution of the phosphorus content in the obtained ingot, the formulas for the estimation of the phosphorus content in silicon is developed and the removal rate of phosphorus is calculated to be over 80%. Phosphorus in silicon could be effectively removed by evaporation when the beam density is over 235mA.