广东药学
廣東藥學
엄동약학
2001年
1期
18-19
,共2页
高效液相色谱法%黄芩苷%小柴胡片
高效液相色譜法%黃芩苷%小柴鬍片
고효액상색보법%황금감%소시호편
用高效液相色谱法对小柴胡片中的黄芩苷进行含量测定，采用Shimpack-C18柱，以磷酸二氢铵溶液-甲醇为流动相，检测波长为278nm，对照品在1.608～8.040μg/ml内呈线性关系，r=0.9998，加样回收率平均为99.2%，平均RSD=0.9%。
用高效液相色譜法對小柴鬍片中的黃芩苷進行含量測定，採用Shimpack-C18柱，以燐痠二氫銨溶液-甲醇為流動相，檢測波長為278nm，對照品在1.608～8.040μg/ml內呈線性關繫，r=0.9998，加樣迴收率平均為99.2%，平均RSD=0.9%。
용고효액상색보법대소시호편중적황금감진행함량측정，채용Shimpack-C18주，이린산이경안용액-갑순위류동상，검측파장위278nm，대조품재1.608～8.040μg/ml내정선성관계，r=0.9998，가양회수솔평균위99.2%，평균RSD=0.9%。
Objective:To establish a HPLC method for the determination ofbaicalin in Xiao Chai Hu tablets.Method:The reversed C18column was used.The mobile phase consisted of buffer NH4H2PO4(pH3.0)-Methanol(40:60).The detective wave range was 278nm,Results:The linear range was from 1.608～8.040μg/ml,r=0.9998,the mean recovery was 99.2%,with RSD=0.9%.Conclusions:The method can be used in the determination of baicalin in Xiao Chai Hu tablets.
