CAJ | 학술논문

建立了食品中苏丹橙G、二甲基黄、苏丹黑B非法色素的固相萃取超高效液相串联质谱测定方法。以10%乙醇的丙酮溶液作为提取溶剂,利用MAX强阴离子交换固相萃取柱对样品进行净化。检出限苏丹橙G、二甲基黄为1.0μg/kg,苏丹黑B为10μg/kg。线性范围苏丹橙G、二甲基黄为2.5-2500μg/kg,苏丹黑B为25-25000μg/kg,加标回收为78%～105%。本方法灵敏、准确高效,可对非法油溶色素进行测定及确证。
건립료식품중소단등G、이갑기황、소단흑B비법색소적고상췌취초고효액상천련질보측정방법。이10%을순적병동용액작위제취용제,이용MAX강음리자교환고상췌취주대양품진행정화。검출한소단등G、이갑기황위1.0μg/kg,소단흑B위10μg/kg。선성범위소단등G、이갑기황위2.5-2500μg/kg,소단흑B위25-25000μg/kg,가표회수위78%～105%。본방법령민、준학고효,가대비법유용색소진행측정급학증。
To established a method for simultaneous determination of Sudan orange G,Dimethyl yellow,Sudan black B in food by solid-phase extraction and ultra performance liquid chromatography electrospray ionization-tandem mass spectrometry（SPE-UPLC-MS/MS） method.The samples were extracted by acetone containing 10 % ethanol and cleaned-up by MAX solid phase extraction column.The qualitative detection limits of the method for Sudan Orange G,Dimethyl yellow were 1.0 μg/kg and for Sudan black B was 10 μg/kg.The linear range were 2.5-2500 μg/kg for Sudan orange G,Dimethyl yellow were 1.0 μg/kg and for Sudan black B was 10 μg/kg.The average recoveries of adding standard were 78 %～105 %.The method is sensitive,accurate and could be used for detecting 3 kinds of oil-soluable illegal pigments in food.