稀有金属材料与工程
稀有金屬材料與工程
희유금속재료여공정
RARE METAL MATERIALS AND ENGINEERNG
2010年
z1期
117-121
,共5页
冷文秀%田文怀%高红叶%成生伟
冷文秀%田文懷%高紅葉%成生偉
랭문수%전문부%고홍협%성생위
析出%时效硬化%B2晶体结构%相变
析齣%時效硬化%B2晶體結構%相變
석출%시효경화%B2정체결구%상변
precipitation%age-hardening%B2 crystal structure%phase transformation
研究了不同成分的Fe-Cu二元合金在过饱和固溶体状态下晶粒尺寸和硬度之间的关系,分析了Cu元素的固溶强化作用.研究了Fe-Cu二元合金的时效硬化现象和Cu元素的析出过程.结果表明Fe-Cu二元合金硬度值增加近一倍.通过透射电镜观察到随时效时间的增加,析出相的尺寸逐渐增大,形状由球形变为棒状.电子衍射花样分析得知,时效处理硬度达到最大值时对应的析出相具有B2型晶体结构,与基体之间保持平行位向关系.透射电镜观察到位错与析出相之间存在典型的引力型交互作用,由于软析出相对运动位错的钉扎效应而使Fe-Cu二元合金得到有效强化.
研究瞭不同成分的Fe-Cu二元閤金在過飽和固溶體狀態下晶粒呎吋和硬度之間的關繫,分析瞭Cu元素的固溶彊化作用.研究瞭Fe-Cu二元閤金的時效硬化現象和Cu元素的析齣過程.結果錶明Fe-Cu二元閤金硬度值增加近一倍.通過透射電鏡觀察到隨時效時間的增加,析齣相的呎吋逐漸增大,形狀由毬形變為棒狀.電子衍射花樣分析得知,時效處理硬度達到最大值時對應的析齣相具有B2型晶體結構,與基體之間保持平行位嚮關繫.透射電鏡觀察到位錯與析齣相之間存在典型的引力型交互作用,由于軟析齣相對運動位錯的釘扎效應而使Fe-Cu二元閤金得到有效彊化.
연구료불동성분적Fe-Cu이원합금재과포화고용체상태하정립척촌화경도지간적관계,분석료Cu원소적고용강화작용.연구료Fe-Cu이원합금적시효경화현상화Cu원소적석출과정.결과표명Fe-Cu이원합금경도치증가근일배.통과투사전경관찰도수시효시간적증가,석출상적척촌축점증대,형상유구형변위봉상.전자연사화양분석득지,시효처리경도체도최대치시대응적석출상구유B2형정체결구,여기체지간보지평행위향관계.투사전경관찰도위착여석출상지간존재전형적인력형교호작용,유우연석출상대운동위착적정찰효응이사Fe-Cu이원합금득도유효강화.
The relationship between the grain size and hardness for binary Fe-Cu alloys with different chemical compositions was investigated under the condition of supersaturation. The solid solution hardening of Cu element in the binary Fe-Cu alloys has been investigated in this study. The aging hardening phenomenon and precipitation behavior have been investigated for Fe-Cu binary alloys. Results show that the hardness of Fe-Cu alloys is almost doubled by aging treatment. TEM observation reveals that with prolonging the aging time, the size of the precipitates increases, and the morphology of the precipitates changes from spherical shape to bar-like shape. The electron diffraction analyses show that the precipitate of Cu is of B2 crystal structure corresponding to the peak aging condition. The B2 precipitates keep parallel lattice orientation relationship with the Fe matrix. The observation of interaction between dislocation and precipitates by TEM shows that there exists a typical attractive interaction between the moving dislocation and precipitates. The pinning-up of moving dislocation by soft precipitates prevents the movement of dislocation during deformation and provides strengthening in Fe-Cu binary alloys.