光谱实验室
光譜實驗室
광보실험실
CHINESE JOURNAL OF SPECTROSCOPY LABORATORY
2010年
1期
197-201
,共5页
肖杭%黎云祥%蔡凌云%高侠%何理
肖杭%黎雲祥%蔡凌雲%高俠%何理
초항%려운상%채릉운%고협%하리
白簕%总黄酮%超声波辅助提取%正交试验
白簕%總黃酮%超聲波輔助提取%正交試驗
백륵%총황동%초성파보조제취%정교시험
Acanthopanan THfoliatus%Total Flavones%Ultrasonic Extraction%Orthogonal Test
采用超声辅助法提取白簕茎皮中总黄酮化合物,通过单因素试验和正交试验,研究了超声提取条件(超声功率,乙醇浓度,料液比,时间)对其中总黄酮提取的影响.白簕荃皮总黄酮最佳提取工艺为:料液比1:30,乙醇浓度70%,超声功率120W,提取时间25min,在此工艺条件下提取,总黄酮含量为53.0843mg/g.
採用超聲輔助法提取白簕莖皮中總黃酮化閤物,通過單因素試驗和正交試驗,研究瞭超聲提取條件(超聲功率,乙醇濃度,料液比,時間)對其中總黃酮提取的影響.白簕荃皮總黃酮最佳提取工藝為:料液比1:30,乙醇濃度70%,超聲功率120W,提取時間25min,在此工藝條件下提取,總黃酮含量為53.0843mg/g.
채용초성보조법제취백륵경피중총황동화합물,통과단인소시험화정교시험,연구료초성제취조건(초성공솔,을순농도,료액비,시간)대기중총황동제취적영향.백륵전피총황동최가제취공예위:료액비1:30,을순농도70%,초성공솔120W,제취시간25min,재차공예조건하제취,총황동함량위53.0843mg/g.
Total flavones were extracted from the stem bark of Acanthopanan trifoliatus by means of ultrasonic extraction technique.The operation condition,such as power of ultrasonic,the content of ethanol,ultrasonic time and the ratio of sample weight to solvent volume were studied by single factor and orthogonal test.The optimal extraction conditions were obtained as extraction solvent of 70%ethanol,power of ultrasonic 120W,ultrasonic time in 25 min and the ratio of sample weight to solvent volume at 1:30.Under the optimized conditions,the extraction percent of total flavones from stem bark of Acanthopanan trifoliatus is 53.0843mg/g.