CAJ | 학술논문

　　应用气相色谱法/原子发射检测器（ GC/AED）分离检测主流烟气粒相物中的含氮碱性成分。3种类型烟叶（典型烤烟、白肋烟和香料烟）、不同香型烤烟烟叶和成品卷烟经过吸烟机抽吸后，收集主流烟气粒相物。粒相物经过连续萃取和反萃取分离，得到含氮的碱性成分，进行GC/AED检测。结果表明，GC/AED能够检测出主流烟气中吡嗪类、吡啶类和烟草微量生物碱类成分。比较了不同样品含氮成分的异同，结果表明，白肋烟烟叶主流烟气粒相物中含氮成分较多，含量最高，烤烟和香料烟烟叶主流烟气粒相物中含氮成分相对较少，含量较低；不同香型烤烟烟叶主流烟气粒相物中主要含氮成分基本类似；不同品牌卷烟主流烟气粒相物中主要含氮成分基本类似，烤烟型卷烟假木贼碱相对百分含量较高（3.84％～4.62％），而混合型卷烟降烟碱相对百分含量较高（5.22％）。
　　응용기상색보법/원자발사검측기（ GC/AED）분리검측주류연기립상물중적함담감성성분。3충류형연협（전형고연、백륵연화향료연）、불동향형고연연협화성품권연경과흡연궤추흡후，수집주류연기립상물。립상물경과련속췌취화반췌취분리，득도함담적감성성분，진행GC/AED검측。결과표명，GC/AED능구검측출주류연기중필진류、필정류화연초미량생물감류성분。비교료불동양품함담성분적이동，결과표명，백륵연연협주류연기립상물중함담성분교다，함량최고，고연화향료연연협주류연기립상물중함담성분상대교소，함량교저；불동향형고연연협주류연기립상물중주요함담성분기본유사；불동품패권연주류연기립상물중주요함담성분기본유사，고연형권연가목적감상대백분함량교고（3.84％～4.62％），이혼합형권연강연감상대백분함량교고（5.22％）。
Compounds containing N element in particulate matter of mainstream smoke of different tobacco samples were isolated and determined by GC/AED.The particulate matters of mainstream smoke from 3 types of tobacco leaves ( typical flue-cured tobacco leaf , burley tobacco leaf and orien-tal tobacco leaf ) , different flavor flue-cured tobacco leaves and cigarettes with different brands were collected through smoking machine .The particulate matter was successively extracted with different solvents.Then alkaline extractants containing N element were collected and determined by GC /AED.The results showed that the derivatives of pyrazine , pyridine and tobacco trace alkaloids could be detected by GC/AED.The compounds containing N element in different samples were compared .The kinds and amount of compounds containing N element in the particulate matter of mainstream smoke of burley tobacco leaf were more than those in flue-cured tobacco and oriental tobacco leaves . The kinds and amount of compounds containing N element in the particulate matter of mainstream smoke of different flavor tobacco leaves were similar .And those in cigarettes with different brands were also similar .However , there were more anabasine ( 3.84%~4.62%) in flue-cured cigarette and more nornicotine (5.22%) in blended type cigarette .