西部林业科学
西部林業科學
서부임업과학
JOURNAL OF WEST CHINA FORESTRY SCIENCE
2014年
3期
27-30
,共4页
李军集%周丽珠%聂永雄%舒文波%梁忠云%谷瑶
李軍集%週麗珠%聶永雄%舒文波%樑忠雲%穀瑤
리군집%주려주%섭영웅%서문파%량충운%곡요
马尾松%土贡种源%松针油%GC-MS
馬尾鬆%土貢種源%鬆針油%GC-MS
마미송%토공충원%송침유%GC-MS
Pinus massoniana%Tugong Provenance%pine needle oil%GC-MS
用挥发油提取器提取马尾松土贡种源松针中挥发油,利用气相色谱-质谱( GC-MS)分析其中的化学成分,采用GC峰面积归一化法定量,并与马尾松普通种源松针油做对比。结果表明,土贡种源和普通种源挥发油得油率分别为0.52%、0.60%,各分出69、75个成分,鉴定其中23个,分别占挥发油总量的92.65%、94.56%,其挥发油主要成分为α-蒎烯(37.673%、46.715%)、莰烯(3.724%、3.015%)、β-蒎烯(14.969%、12.978%)、石竹烯(8.242%、10.212%),除α-蒎烯含量相差9.042%以外,其他成分含量相差不大。
用揮髮油提取器提取馬尾鬆土貢種源鬆針中揮髮油,利用氣相色譜-質譜( GC-MS)分析其中的化學成分,採用GC峰麵積歸一化法定量,併與馬尾鬆普通種源鬆針油做對比。結果錶明,土貢種源和普通種源揮髮油得油率分彆為0.52%、0.60%,各分齣69、75箇成分,鑒定其中23箇,分彆佔揮髮油總量的92.65%、94.56%,其揮髮油主要成分為α-蒎烯(37.673%、46.715%)、莰烯(3.724%、3.015%)、β-蒎烯(14.969%、12.978%)、石竹烯(8.242%、10.212%),除α-蒎烯含量相差9.042%以外,其他成分含量相差不大。
용휘발유제취기제취마미송토공충원송침중휘발유,이용기상색보-질보( GC-MS)분석기중적화학성분,채용GC봉면적귀일화법정량,병여마미송보통충원송침유주대비。결과표명,토공충원화보통충원휘발유득유솔분별위0.52%、0.60%,각분출69、75개성분,감정기중23개,분별점휘발유총량적92.65%、94.56%,기휘발유주요성분위α-파희(37.673%、46.715%)、감희(3.724%、3.015%)、β-파희(14.969%、12.978%)、석죽희(8.242%、10.212%),제α-파희함량상차9.042%이외,기타성분함량상차불대。
The essential oil of Tugong Provenance and ordinary type Pinus massoniana was extracted by the volatile oil extractor , and the chemical composition of essential oil was analyzed and compared by gas chromatography -mass spectrometry ( GC-MS) by using the peak area normalization method .The results showed that the yield of essential oil of these two provenances were 0.52 % and 0.60 % respectively .23 constituents were identified from 69 and 75 chromatographic peaks respectively , and the relative content up to 92.65%, 94.56% respectively .The ma-jor constituents were α-pinene ( 37.673 %, 46.715 %) , camphene ( 3.724 %, 3.015 %) , β-pinene (14.969 %, 12.978 %), caryophyllene (8.242 %, 10.212 %).The major constituents were similar except theα-pinene content difference with 9.042 %.