中国有色金属学报
中國有色金屬學報
중국유색금속학보
THE CHINESE JOURNAL OF NONFERROUS METALS
2013年
8期
2176-2181
,共6页
茹祥坤%刘廷光%夏爽%周邦新%马爱利%郑玉贵
茹祥坤%劉廷光%夏爽%週邦新%馬愛利%鄭玉貴
여상곤%류정광%하상%주방신%마애리%정옥귀
晶界工程%晶界特征分布%晶粒团簇%白铜合金
晶界工程%晶界特徵分佈%晶粒糰簇%白銅閤金
정계공정%정계특정분포%정립단족%백동합금
grain boundary engineering%grain boundary distribution character%grain-cluster%cupronickel alloy
研究晶界工程处理过程中的冷轧变形量和再结晶退火对白铜B10合金晶界特征分布的影响,采用电子背散射衍射(EBSD)技术表征分析晶界网络的变化。结果表明:白铜B10合金经冷轧7%后在800℃退火10 min可使低ΣCSL(Coincidence site lattice,Σ≤29)晶界比例提高到75%以上,同时形成尺寸较大的“互有Σ3n取向关系晶粒的团簇”显微组织。当变形量小于7%时,经800℃退火后没有完全再结晶;当变形量大于7%时,低ΣCSL晶界比例和平均晶粒团簇的尺寸随冷轧变形量的增加而下降。
研究晶界工程處理過程中的冷軋變形量和再結晶退火對白銅B10閤金晶界特徵分佈的影響,採用電子揹散射衍射(EBSD)技術錶徵分析晶界網絡的變化。結果錶明:白銅B10閤金經冷軋7%後在800℃退火10 min可使低ΣCSL(Coincidence site lattice,Σ≤29)晶界比例提高到75%以上,同時形成呎吋較大的“互有Σ3n取嚮關繫晶粒的糰簇”顯微組織。噹變形量小于7%時,經800℃退火後沒有完全再結晶;噹變形量大于7%時,低ΣCSL晶界比例和平均晶粒糰簇的呎吋隨冷軋變形量的增加而下降。
연구정계공정처리과정중적랭알변형량화재결정퇴화대백동B10합금정계특정분포적영향,채용전자배산사연사(EBSD)기술표정분석정계망락적변화。결과표명:백동B10합금경랭알7%후재800℃퇴화10 min가사저ΣCSL(Coincidence site lattice,Σ≤29)정계비례제고도75%이상,동시형성척촌교대적“호유Σ3n취향관계정립적단족”현미조직。당변형량소우7%시,경800℃퇴화후몰유완전재결정;당변형량대우7%시,저ΣCSL정계비례화평균정립단족적척촌수랭알변형량적증가이하강。
The effects of cold rolling deformation and annealing on the grain boundary character distribution (GBCD) during grain boundary engineering (GBE) treatment were investigated by electron backscatter diffraction (EBSD) in cupronickel B10 alloy. The results show that the proportion of low-Σ CSL (Coincidence site lattice, Σ≤29) grain boundaries increase to more than 75% by 7% cold rolling and subsequent annealing at 800 ℃. In this case, the grain boundary network (GBN) is featured by the formation of highly twinned large size grain-clusters produced by multiple twinning during recrystallization. When the cold rolling deformation amount is less than 7%, the 800℃annealing can not induce perfect recrystallization. The perfect recrystallization occurs when the deformation amount is more than 7%, and the proportion of low-ΣCSL grain boundaries and the average size of grain-clusters decrease with the increase of the cold rolling reduction ratio.