西北药学杂志
西北藥學雜誌
서북약학잡지
2013年
5期
478-480
,共3页
朱宇红%马玉芳%鲍和%任璐%井航%赵桂兰%王军宪
硃宇紅%馬玉芳%鮑和%任璐%井航%趙桂蘭%王軍憲
주우홍%마옥방%포화%임로%정항%조계란%왕군헌
狭叶米口袋%米口袋属%化学成分
狹葉米口袋%米口袋屬%化學成分
협협미구대%미구대속%화학성분
Gueldenstaedtia stenophylla Bunge%Gueldenstaedtia Fisch%chemical constituents
目的对狭叶米口袋的正丁醇部分进行化学成分研究。方法采用正相硅胶、反相硅胶、聚酰胺柱层析进行分离纯化,根据理化性质和光谱分析鉴定化合物结构。结果从狭叶米口袋正丁醇部分中分离鉴定了4个化合物,分别为β-谷甾醇(1)、槲皮素-3-O-β-D-葡萄糖苷(2)、胡萝卜苷(3)和大豆苷元B-3-O-[α-D-鼠李糖基(1→2)-β-D-葡萄糖基(1→2)-β-D-葡萄糖醛酸苷(4)。结论化合物2和4分别为黄酮类和三萜皂苷类化合物,是首次从狭叶米口袋中分离得到。
目的對狹葉米口袋的正丁醇部分進行化學成分研究。方法採用正相硅膠、反相硅膠、聚酰胺柱層析進行分離純化,根據理化性質和光譜分析鑒定化閤物結構。結果從狹葉米口袋正丁醇部分中分離鑒定瞭4箇化閤物,分彆為β-穀甾醇(1)、槲皮素-3-O-β-D-葡萄糖苷(2)、鬍蘿蔔苷(3)和大豆苷元B-3-O-[α-D-鼠李糖基(1→2)-β-D-葡萄糖基(1→2)-β-D-葡萄糖醛痠苷(4)。結論化閤物2和4分彆為黃酮類和三萜皂苷類化閤物,是首次從狹葉米口袋中分離得到。
목적대협협미구대적정정순부분진행화학성분연구。방법채용정상규효、반상규효、취선알주층석진행분리순화,근거이화성질화광보분석감정화합물결구。결과종협협미구대정정순부분중분리감정료4개화합물,분별위β-곡치순(1)、곡피소-3-O-β-D-포도당감(2)、호라복감(3)화대두감원B-3-O-[α-D-서리당기(1→2)-β-D-포도당기(1→2)-β-D-포도당철산감(4)。결론화합물2화4분별위황동류화삼첩조감류화합물,시수차종협협미구대중분리득도。
Objective To research the chemical constituents of the n-butyl alcohol part of Gueldenstaedtia stenophylla Bunge . Method The n-butyl alcohol fraction of Gueldenstaedtia stenophylla Bunge was separated and purified by silica gel ,ODS and poly amide column chromatography .The physicochemical property and spectral analysis were used to analyze the compound structures . Results Four compounds were obtained ,and they were identified as β-sitosterol (1) ,quercetin-3-O-β-D-glucoside (2) ,β-sitosterol glucoside (3) ,and soyabean saponin B-3-O-[α-D-rhamnose (1→2)-β-D-glucose (1→2)-β-D-glucuronic] (4) .Conclusion Com-pound 2 ,4 were flavanoid and triterpenoid saponin .These compounds were isolated for the first time from Gueldenstaedtia steno-phylla Bunge .