西北药学杂志
西北藥學雜誌
서북약학잡지
2013年
5期
466-469
,共4页
何悦%肖会敏%李予蓉%谢艳华%王四旺
何悅%肖會敏%李予蓉%謝豔華%王四旺
하열%초회민%리여용%사염화%왕사왕
红芪片%质量标准%薄层色谱法%高效液相色谱法
紅芪片%質量標準%薄層色譜法%高效液相色譜法
홍기편%질량표준%박층색보법%고효액상색보법
Hongqi Tablets%quality standard%TLC%HPLC
目的建立红芪片的质量标准。方法采用TLC法对制剂中黄芪甲苷、黄芪与沙棘药材进行薄层鉴别；采用 HPLC法测定制剂中红景天苷的含量。结果黄芪甲苷、黄芪与沙棘药材的薄层鉴别具有较好的专属性；红景天苷的回归方程：y＝2291627 x＋13360，r＝0．9999，线性范围为0．064～0．960 mg · mL -1；平均回收率为98．5％，RSD值为0．7％。结论所建立的标准可用于该制剂的质量控制。
目的建立紅芪片的質量標準。方法採用TLC法對製劑中黃芪甲苷、黃芪與沙棘藥材進行薄層鑒彆；採用 HPLC法測定製劑中紅景天苷的含量。結果黃芪甲苷、黃芪與沙棘藥材的薄層鑒彆具有較好的專屬性；紅景天苷的迴歸方程：y＝2291627 x＋13360，r＝0．9999，線性範圍為0．064～0．960 mg · mL -1；平均迴收率為98．5％，RSD值為0．7％。結論所建立的標準可用于該製劑的質量控製。
목적건립홍기편적질량표준。방법채용TLC법대제제중황기갑감、황기여사극약재진행박층감별；채용 HPLC법측정제제중홍경천감적함량。결과황기갑감、황기여사극약재적박층감별구유교호적전속성；홍경천감적회귀방정：y＝2291627 x＋13360，r＝0．9999，선성범위위0．064～0．960 mg · mL -1；평균회수솔위98．5％，RSD치위0．7％。결론소건립적표준가용우해제제적질량공제。
Objective To establish and study the quality standard for Hongqi Tablets .Methods Astragaloside ,Astragalus mong-holicus and Hippophae rhamnoides in the preparation were identified by TLC ,respectively .The content of salidroside in the preparation was determined by HPLC .Results The TLC of astragaloside ,Astragalus mongholicus and Hippophae rhamnoides showed good specificity .Salidroside regression equation was y=2 291 627x+13 360 and r=0 .999 9 in the concentration range of 0 .064-0 .960 mg · mL -1 .The average recovery was 98 .5% ,and its RSD was 0 .7% .Conclusion The standard can be used for the preparation quality control .
