CAJ | 학술논문

目的建立克疣纳米乳中冰片、薄荷脑的气相色谱测定方法。方法 HP-5毛细管柱(30 m×320μm×0.25μm),氮气为载气,FID 检测器,进样口温度为230℃。结果冰片、薄荷脑分离度良好,冰片在0.337～1.685μg 范围内线性关系良好,r2＝0.9982,平均回收率为97.5%；薄荷脑在0.234～1.17μg 范围内线性关系良好,r2＝0.9974,平均回收率为97.0%。结论该法简便、准确,可用于克疣纳米乳中冰片、薄荷脑的测定。
목적건립극우납미유중빙편、박하뇌적기상색보측정방법。방법 HP-5모세관주(30 m×320μm×0.25μm),담기위재기,FID 검측기,진양구온도위230℃。결과빙편、박하뇌분리도량호,빙편재0.337～1.685μg 범위내선성관계량호,r2＝0.9982,평균회수솔위97.5%；박하뇌재0.234～1.17μg 범위내선성관계량호,r2＝0.9974,평균회수솔위97.0%。결론해법간편、준학,가용우극우납미유중빙편、박하뇌적측정。
Objective To establish the determination method synthetic borneol and menthol in Keyou nanoemulsion. Methods HP-5 quartz capillary column (30 m×320 μm×0.25 μm) was used with nitrogen as the carrier gas, and FID as the detector. The temperature of the entrance of the capillary vessel column was at 230 ℃. Results Synthetic borneol and menthol in Keyou nanoemulsion were separated well. The calibration curves of synthetic borneol was obtained with good linear relationship within the range of 0.337-1.685 μg (r 2=0.998 2), the average recovery was 97.5%. The calibration curves of menthol was also obtained with a good linear relationship within the range of 0.234-1.17 μg (r 2=0.997 4), the average recovery was 97.0%. Conclusion The methord is simple and accurate. It can be used to control the quality of Keyou nanoemulsion.