CAJ | 학술논문

以 NH4 F为电解质，分别以乙二醇，去离子水为电解液，用阳极氧化法制备了 TiO2纳米管，考察了不同的电解液，电压，阳极氧化时间，电解质浓度等因素对 TiO2纳米管形貌的影响，采用场发射扫描电子显微镜(SEM)对纳米管的形貌和结构进行表征，结果表明：乙二醇制备的纳米管比水基电解液排列有序，管径一致，管径更小；提高电压可使管状更加清晰；增长电解时间，更有利于纳米管的伸长；电解液浓度升高，腐蚀速率增高，会使管长降低。
이 NH4 F위전해질，분별이을이순，거리자수위전해액，용양겁양화법제비료 TiO2납미관，고찰료불동적전해액，전압，양겁양화시간，전해질농도등인소대 TiO2납미관형모적영향，채용장발사소묘전자현미경(SEM)대납미관적형모화결구진행표정，결과표명：을이순제비적납미관비수기전해액배렬유서，관경일치，관경경소；제고전압가사관상경가청석；증장전해시간，경유리우납미관적신장；전해액농도승고，부식속솔증고，회사관장강저。
Used NH4 F as the electrlyote in ethylene glycol and water,prepared TiO2 nanotubes which orderly arranged by anodic oxidation.We Investigated the Influence of Different electrolyte,voltage, anodization time,electrolyte concentration,and other factors on the morphology of TiO2 nanotubes. Observed the morphology and structure of the nanotubes by the field emission scanning electron mi-croscope (SEM).The results show that:Nanotubes obtained in the organic electrolyte,uniform diam-eter,arranged in order.