北方药学
北方藥學
북방약학
JOURNAL OF NORTH PHARMACY
2013年
10期
1-4
,共4页
张敏惠%吴怡%曲凤鸣%陈娟%邹本广
張敏惠%吳怡%麯鳳鳴%陳娟%鄒本廣
장민혜%오이%곡봉명%진연%추본엄
珍珠母贝%糖胺聚糖%提取方法%分离方法%气相色谱-质谱法
珍珠母貝%糖胺聚糖%提取方法%分離方法%氣相色譜-質譜法
진주모패%당알취당%제취방법%분리방법%기상색보-질보법
Mother-of-pearl%Gglycosaminoglycans%Extraction method%Separation methods%Gas chromatography-mass spectrometry
目的：对马氏珍珠母贝中提取、分离得到的糖胺聚糖（glycosam inog lycans， GAG）进行化学组分研究。方法：样品经还原、水解和乙酰化，采用气相色谱-质谱法定性测定。结果：测定出马氏珍珠母贝中经提取、分离得到的GAG中的3种主要成分，其骨架结构分别与（硫酸乙酰）肝素、（硫酸）软骨素和透明质酸相符。结论：马氏珍珠母贝中提取分离的糖胺聚糖中含有肝素、软骨素和透明质酸。
目的：對馬氏珍珠母貝中提取、分離得到的糖胺聚糖（glycosam inog lycans， GAG）進行化學組分研究。方法：樣品經還原、水解和乙酰化，採用氣相色譜-質譜法定性測定。結果：測定齣馬氏珍珠母貝中經提取、分離得到的GAG中的3種主要成分，其骨架結構分彆與（硫痠乙酰）肝素、（硫痠）軟骨素和透明質痠相符。結論：馬氏珍珠母貝中提取分離的糖胺聚糖中含有肝素、軟骨素和透明質痠。
목적：대마씨진주모패중제취、분리득도적당알취당（glycosam inog lycans， GAG）진행화학조분연구。방법：양품경환원、수해화을선화，채용기상색보-질보법정성측정。결과：측정출마씨진주모패중경제취、분리득도적GAG중적3충주요성분，기골가결구분별여（류산을선）간소、（류산）연골소화투명질산상부。결론：마씨진주모패중제취분리적당알취당중함유간소、연골소화투명질산。
Objective:To martensite mother-of-pearl extraction, separation, have been the glycosaminoglycans(glycosam inog lycans, GAG)was studied by means of chemical composition. Methods: The sample after reduction , hydrolysis and acetylation, Detecting by means of gas chromatography - mass spectrometry. Results:The determination of a horse's mother-of-pearl integrated by extraction , separation of GAG in the three major components, its skeleton structure, respectively, and the (acetyl sulfate)heparin, hyaluronic acid and chondroitin (sulfuric acid). Conclusion: The extraction and separation of sugars in markov mother -of -pearl glycosaminoglycans containing heparin, hyaluronic acid and chondroitin.
