福建分析测试
福建分析測試
복건분석측시
FUJIAN ANALYSIS & TESTING
2014年
3期
45-47
,共3页
刘利亚%周贻兵%李磊%张卫国
劉利亞%週貽兵%李磊%張衛國
류리아%주이병%리뢰%장위국
居室空气%甲醛%常规和室间质控%AHMT法
居室空氣%甲醛%常規和室間質控%AHMT法
거실공기%갑철%상규화실간질공%AHMT법
Indoor air%Formaldehyde%Routine laboratory test%AHMT spectrophotometry method
目的:探讨居室空气中甲醛AHMT分光光度法的实验室常规和实验室间分析质量控制。方法:空气中甲醛经固相吸附管采集,用淋洗液洗脱后按居住区大气中甲醛卫生检验标准方法(GB/T16129-1995)中AHMT分光光度法进行分析。结果:样品测定的精密度和准确度结果均位于均值-减差控制图和回收率控制图的上下控制限之间,统一发放标准溶液与本实验室自配标准溶液之间的差值<5%。结论:通过实施实验室分析质量控制程序,可了解测定过程中的误差来源及程度,采取相应措施纠正后甲醛测定结果可控制在允许的置信水平内。
目的:探討居室空氣中甲醛AHMT分光光度法的實驗室常規和實驗室間分析質量控製。方法:空氣中甲醛經固相吸附管採集,用淋洗液洗脫後按居住區大氣中甲醛衛生檢驗標準方法(GB/T16129-1995)中AHMT分光光度法進行分析。結果:樣品測定的精密度和準確度結果均位于均值-減差控製圖和迴收率控製圖的上下控製限之間,統一髮放標準溶液與本實驗室自配標準溶液之間的差值<5%。結論:通過實施實驗室分析質量控製程序,可瞭解測定過程中的誤差來源及程度,採取相應措施糾正後甲醛測定結果可控製在允許的置信水平內。
목적:탐토거실공기중갑철AHMT분광광도법적실험실상규화실험실간분석질량공제。방법:공기중갑철경고상흡부관채집,용림세액세탈후안거주구대기중갑철위생검험표준방법(GB/T16129-1995)중AHMT분광광도법진행분석。결과:양품측정적정밀도화준학도결과균위우균치-감차공제도화회수솔공제도적상하공제한지간,통일발방표준용액여본실험실자배표준용액지간적차치<5%。결론:통과실시실험실분석질량공제정서,가료해측정과정중적오차래원급정도,채취상응조시규정후갑철측정결과가공제재윤허적치신수평내。
Purpose This paper will discuss indoor formaldehyde AHMT spectrophotometry routine laboratory test and inter-laboratory analytical quality control. Method Formaldehyde, collected by solid phase adsorption tube and eluted with eluent, analysis by AHMT spectrophotometry of Formaldehyde in air of residential areas health inspection standard method(GB/T16129-1995). Result The results of precision and accuracy are between the upper and lower control limits of the mean-range charts and recovery control charts. The difference between uniform standard solution and the laboratory standard solution is less than 5%. Conclusion Through the implementation of laboratory analytical quality control procedures, we can understand the process of measuring the degree of error sources and take appropriate measures to correct measurement results controlled within the allowable level of confidence.