山东冶金
山東冶金
산동야금
SHANDONG METALLURY
2014年
4期
44-47
,共4页
傅士刚%王俊秀%张小燕%王艳芹%魏新晖
傅士剛%王俊秀%張小燕%王豔芹%魏新暉
부사강%왕준수%장소연%왕염근%위신휘
高速钢轧辊%滴定法%光度法%联合快速测定
高速鋼軋輥%滴定法%光度法%聯閤快速測定
고속강알곤%적정법%광도법%연합쾌속측정
high-speed steel roll%titration%spectrophotometry method%rapid united determination
用磷酸、高氯酸统一溶解处理方法制备试液，用同一母液分别以光度法和滴定法测定W、Mn、Mo、Co、Cu、V、Cr元素的含量。通过控制测定的酸度，各元素线性良好，W、Mn、Mo、Co、Cu、V、Cr的RSD分别≤1.42%、≤1.26%、≤2.12%、≤6.72%、≤5.73%、≤3.53%、≤1.53%。该方法缩短了分析周期，精密度和准确度高，能够满足快速测定的要求。
用燐痠、高氯痠統一溶解處理方法製備試液，用同一母液分彆以光度法和滴定法測定W、Mn、Mo、Co、Cu、V、Cr元素的含量。通過控製測定的痠度，各元素線性良好，W、Mn、Mo、Co、Cu、V、Cr的RSD分彆≤1.42%、≤1.26%、≤2.12%、≤6.72%、≤5.73%、≤3.53%、≤1.53%。該方法縮短瞭分析週期，精密度和準確度高，能夠滿足快速測定的要求。
용린산、고록산통일용해처리방법제비시액，용동일모액분별이광도법화적정법측정W、Mn、Mo、Co、Cu、V、Cr원소적함량。통과공제측정적산도，각원소선성량호，W、Mn、Mo、Co、Cu、V、Cr적RSD분별≤1.42%、≤1.26%、≤2.12%、≤6.72%、≤5.73%、≤3.53%、≤1.53%。해방법축단료분석주기，정밀도화준학도고，능구만족쾌속측정적요구。
The test solution was prepared by phosphoric acid and perchloric acid dissolution method, then to take same solution, the photometric method and titration method were respectively used to determine the contents of W, Mn, Mo, Co, Cu, V and Cr elements. By controlling the acidity during determination, the linear of each element was good. The method has shortened the cycle, high precision and accuracy of the analysis. RSD of W, Mn, Mo, Co, Cu, V and Cr were separately less than or equal to 1.42%, 1.26%, 2.12%, 6.72%, 5.73%, 3.53%, 1.53%, being able to meet the requirements of rapid determination.
