CAJ | 학술논문

为了提高同时测定食品中砷、硒和汞3种元素含量的速度，采用一次性消解样品后用HG-AFS法连续完成测定食品中3种元素含量的新方法。在选定的最佳试验条件下测得Se、As、Hg的RSD分别为：3.7%，2.8%，和4.7%；回收率分别为：95.0%、102.0%和91.9%；采用该法和国标法对同一样品进行比较测定，结果经t值检验P>0.05，差别无显著性。该法具有快速、简单、准确性好，和国标法分别消解样品相比，有一次性消解样品，可连续完成测定3种元素含量，操作简单,快速，节省试剂，工作效率高等优点，值得推广应用。
위료제고동시측정식품중신、서화홍3충원소함량적속도，채용일차성소해양품후용HG-AFS법련속완성측정식품중3충원소함량적신방법。재선정적최가시험조건하측득Se、As、Hg적RSD분별위：3.7%，2.8%，화4.7%；회수솔분별위：95.0%、102.0%화91.9%；채용해법화국표법대동일양품진행비교측정，결과경t치검험P>0.05，차별무현저성。해법구유쾌속、간단、준학성호，화국표법분별소해양품상비，유일차성소해양품，가련속완성측정3충원소함량，조작간단,쾌속，절성시제，공작효솔고등우점，치득추엄응용。
The aim was to improve the efficiency of measuring the weight of Se, As and Hg in food. The continuous determination of one-time digestion was used to measure the weight of Arsenic, Selenium and Mercury in food. Under selected best experimental environment, the RSD of Se, As, Hg were measured as 3.7%, 2.8% and 4.7% respectively; the recovery rates were measured as 95.0%, 102.0% and 91.9%. When applied this method and National Standard Method to measure the same sample, there was no significant difference between two results as both results’t-value test showed P>0.05. This new method was fast, simple and accurate. Compared to National Standard Method, when disposable digestion samples were available, the measurement of three elements could be done continuously. It only required simple, fast operations and also reduced reagent consumption. The above-mentioned advantages made it worthy of promotion and use.