唐山师范学院学报
唐山師範學院學報
당산사범학원학보
JOURNAL OF TANGSHAN TEACHERS COLLEGE
2013年
5期
5-9
,共5页
刘征原%廉志红%张铁莉%于翠
劉徵原%廉誌紅%張鐵莉%于翠
류정원%렴지홍%장철리%우취
太阳光%纳米银溶胶%荧光素%荧光增强
太暘光%納米銀溶膠%熒光素%熒光增彊
태양광%납미은용효%형광소%형광증강
sunlight%nano-silver sol%fluorescein%fluorescence enhancement
以太阳为光源,以硝酸银和柠檬酸三钠为反应试剂、聚乙烯吡咯烷酮为保护剂,通过控制光照时间和光照强度,制备了蓝色和红色纳米银溶胶,比较了两种不同颜色纳米银溶胶形成过程的U V-Vi s吸收光谱;采用 U V-Vi s 分光光度法和荧光法研究了荧光素和两种颜色纳米银溶胶的相互作用。实验发现,纳米银的加入使得荧光素的吸收峰红移,并使得荧光素荧光增强。
以太暘為光源,以硝痠銀和檸檬痠三鈉為反應試劑、聚乙烯吡咯烷酮為保護劑,通過控製光照時間和光照彊度,製備瞭藍色和紅色納米銀溶膠,比較瞭兩種不同顏色納米銀溶膠形成過程的U V-Vi s吸收光譜;採用 U V-Vi s 分光光度法和熒光法研究瞭熒光素和兩種顏色納米銀溶膠的相互作用。實驗髮現,納米銀的加入使得熒光素的吸收峰紅移,併使得熒光素熒光增彊。
이태양위광원,이초산은화저몽산삼납위반응시제、취을희필각완동위보호제,통과공제광조시간화광조강도,제비료람색화홍색납미은용효,비교료량충불동안색납미은용효형성과정적U V-Vi s흡수광보;채용 U V-Vi s 분광광도법화형광법연구료형광소화량충안색납미은용효적상호작용。실험발현,납미은적가입사득형광소적흡수봉홍이,병사득형광소형광증강。
Under the irradiation of sunlight blue and red colours of nano-silver sols were prepared by controlling the intensity and the irradiation time using silver nitrate and trisodium citrate as the reactants and polyvinylpyrrolidone as the capping agent. The ultraviolet-visible absorption (UV-Vis) spectra were monitored and compared during the evolution of the two colour nano-silver sols. And the interactions of fluorescein with the nano-silver sols were investigated by UV-Vis spectrometry and fluorescence photometry, respectively. It was found that the absorbance and fluorescence intensity of fluorescein was enhanced and the peak position of the UV-Vis spectrum had a red shift compared with that of fluorescein itself on adding nano-silver sols into the FL solutions.