磁性材料及器件
磁性材料及器件
자성재료급기건
JOURNAL OF MAGNETIC MATERIALS AND DEVICES
2013年
5期
70-72,79
,共4页
李志杰%吕犇%于忠淇%田鸣%李旭%赵骞
李誌傑%呂犇%于忠淇%田鳴%李旭%趙鶱
리지걸%려분%우충기%전명%리욱%조건
锶铁氧体%纳米添加剂%陶瓷法%磁性能
鍶鐵氧體%納米添加劑%陶瓷法%磁性能
송철양체%납미첨가제%도자법%자성능
strontium ferrite%nano-additive%ceramic process%magnetic performance
为了改善锶铁氧体在磁选设备和衬板中的应用,提高锶铁氧体磁性能和力学性能,以永磁铁氧体预烧料(SrFe12O19)作为原料,添加葡萄糖酸钙、CaCO3、Al2O3、SiO2,在烧结温度1240℃、恒温2h条件下,采用陶瓷法制备锶铁氧体,并用扫描电镜、磁性测试仪、维氏硬度计、X 射线衍射仪等对样品性能进行检测和物相分析。结果表明,对于葡萄糖酸钙(0.3wt%)、CaCO3(0.5wt%)、Al2O3(0.5wt%)、SiO2(0.3wt%)的组合添加,样品性能较优:Br=406.7mT,Hcj=336.7kA/m,(BH)max=35.58kJ/m3。合适的添加剂种类、剂量及纳米化提高了磁性相的取向度,改善了磁体的综合磁性能和力学性能。
為瞭改善鍶鐵氧體在磁選設備和襯闆中的應用,提高鍶鐵氧體磁性能和力學性能,以永磁鐵氧體預燒料(SrFe12O19)作為原料,添加葡萄糖痠鈣、CaCO3、Al2O3、SiO2,在燒結溫度1240℃、恆溫2h條件下,採用陶瓷法製備鍶鐵氧體,併用掃描電鏡、磁性測試儀、維氏硬度計、X 射線衍射儀等對樣品性能進行檢測和物相分析。結果錶明,對于葡萄糖痠鈣(0.3wt%)、CaCO3(0.5wt%)、Al2O3(0.5wt%)、SiO2(0.3wt%)的組閤添加,樣品性能較優:Br=406.7mT,Hcj=336.7kA/m,(BH)max=35.58kJ/m3。閤適的添加劑種類、劑量及納米化提高瞭磁性相的取嚮度,改善瞭磁體的綜閤磁性能和力學性能。
위료개선송철양체재자선설비화츤판중적응용,제고송철양체자성능화역학성능,이영자철양체예소료(SrFe12O19)작위원료,첨가포도당산개、CaCO3、Al2O3、SiO2,재소결온도1240℃、항온2h조건하,채용도자법제비송철양체,병용소묘전경、자성측시의、유씨경도계、X 사선연사의등대양품성능진행검측화물상분석。결과표명,대우포도당산개(0.3wt%)、CaCO3(0.5wt%)、Al2O3(0.5wt%)、SiO2(0.3wt%)적조합첨가,양품성능교우:Br=406.7mT,Hcj=336.7kA/m,(BH)max=35.58kJ/m3。합괄적첨가제충류、제량급납미화제고료자성상적취향도,개선료자체적종합자성능화역학성능。
In order to improve applications of strontium ferrite in magnetic separation equipment and lining board, using presintered SrFe12O19 as starting materials, and adding calcium gluconate, CaCO3, Al2O3, SiO2, strontim ferrite was prepared by ceramic process. The sample was characterized by scanning electron microscope, magnetic material automatic testing equipment, Vickers hardness tester and X-ray diffraction, respectively. The results show that relatively good magnetic property is achieved with Br=406.7mT, Hcj=336.7kA/m, (BH)max=35.58kJ/m3 for sample with combined adding of 0.3wt%calcium gluconate, 0.5wt%CaCO3 , 0.5wt%Al2O3 and 0.3wt%SiO2. As a result of proper kinds and amount of nano-additives, the aligment of magnetic phase, and resultantly the comprehensive magnetic and mechanical properties of the material is improved.