CAJ | 학술논문

通过两步阳极氧化法制得氧化铝模板，然后在氧化铝模板的纳米孔洞中，用微波辅助溶胶-凝胶-模板法制备出Ni纳米线。分别用XRD、TEM 和VSM对样品的相成分、显微结构和磁性进行观察和测量。结果表明，Ni纳米线为面心立方结构，氧化铝模板的孔洞分布均匀，Ni纳米线的直径取决于氧化铝模板纳米孔洞的大小。纳米线具有铁磁性，其易磁化轴平行于纳米线的长轴方向。
통과량보양겁양화법제득양화려모판，연후재양화려모판적납미공동중，용미파보조용효-응효-모판법제비출Ni납미선。분별용XRD、TEM 화VSM대양품적상성분、현미결구화자성진행관찰화측량。결과표명，Ni납미선위면심립방결구，양화려모판적공동분포균균，Ni납미선적직경취결우양화려모판납미공동적대소。납미선구유철자성，기역자화축평행우납미선적장축방향。
Anodic aluminum oxide (AAO) templates with a uniform pore diameter were fabricated using a two-step oxidization method. Then, arrays of Ni nanowires were prepared using AAO template by microwave-assisted sol-gel method. The microstructure, morphology of the samples were characterized by using X-ray diffraction (XRD), transmission electron microscopy (TEM) and vibrating sample magnetometer (VSM), respectively. The XRD results suggest that Ni nanowires with a F.C.C structure were successfully synthesized and TEM studies show the diameters of the nanowires is consistent with the pore size of the AAO template, so the diameter of Ni nanowires is determined by pore size of the AAO template. Also, typical ferromagnetic property is investigated in the Ni nanowires,and the easy magnetization axis is along the long axis of Ni nanowires.