化学研究与应用
化學研究與應用
화학연구여응용
CHEMICAL RESEARCH AND APPLICATION
2013年
8期
1215-1217
,共3页
贾强强%马养民%康永祥%程小伟
賈彊彊%馬養民%康永祥%程小偉
가강강%마양민%강영상%정소위
马蹄香%化学成分%马兜铃内酰胺
馬蹄香%化學成分%馬兜鈴內酰胺
마제향%화학성분%마두령내선알
saruma henryi%chemical constituent%aristololactam
研究马蹄香( Saruma henryi Oliv.)全草的化学成分。采用硅胶柱层析、Sephadex LH-20柱层析,结合重结晶等方法分离纯品化合物,并通过化合物的理化性质和波谱数据鉴定其化学结构。分离并鉴定了6个化合物,分别为马兜铃内酰胺BII(1)、7-甲氧基-马兜铃内酰胺IV(2)、马兜铃内酰胺AII(3)、马兜铃酸I(4)、胡萝卜苷(5)、马兜铃酸IV(6)。化合物1和6为首次从该属植物中分离得到。
研究馬蹄香( Saruma henryi Oliv.)全草的化學成分。採用硅膠柱層析、Sephadex LH-20柱層析,結閤重結晶等方法分離純品化閤物,併通過化閤物的理化性質和波譜數據鑒定其化學結構。分離併鑒定瞭6箇化閤物,分彆為馬兜鈴內酰胺BII(1)、7-甲氧基-馬兜鈴內酰胺IV(2)、馬兜鈴內酰胺AII(3)、馬兜鈴痠I(4)、鬍蘿蔔苷(5)、馬兜鈴痠IV(6)。化閤物1和6為首次從該屬植物中分離得到。
연구마제향( Saruma henryi Oliv.)전초적화학성분。채용규효주층석、Sephadex LH-20주층석,결합중결정등방법분리순품화합물,병통과화합물적이화성질화파보수거감정기화학결구。분리병감정료6개화합물,분별위마두령내선알BII(1)、7-갑양기-마두령내선알IV(2)、마두령내선알AII(3)、마두령산I(4)、호라복감(5)、마두령산IV(6)。화합물1화6위수차종해속식물중분리득도。
The constituents of the whole herb of saruma henryi Oliv.were investigated.The compounds were isolated by silica gel column chromatography ,Sephadex LH-20 column chromatography and purified via recrystallization.Their structures were identified by physicochemical properties and spectra analysis.Six compounds were obtained and identified as aristololactam BII (1),7-methox-yl-aristololactam IV(2),aristololactam AII(3),aristolic acid I(4),daucosterol(5)aristolic acid IV(6).Compound 1 and 6 were obtained from the genus for the first time.