红外与激光工程
紅外與激光工程
홍외여격광공정
INFRARED AND LASER ENGINEERING
2013年
7期
1770-1775
,共6页
刘华松%傅翾%王利栓%姜玉刚%冷健%庄克文%季一勤
劉華鬆%傅翾%王利栓%薑玉剛%冷健%莊剋文%季一勤
류화송%부현%왕리전%강옥강%랭건%장극문%계일근
离子束溅射%Ta2O5薄膜%正交实验%光学常数%沉积速率%应力
離子束濺射%Ta2O5薄膜%正交實驗%光學常數%沉積速率%應力
리자속천사%Ta2O5박막%정교실험%광학상수%침적속솔%응력
ion beam sputterings%Ta2O5 thin film%orthogonal experiment%optical constants%deposition rate%stress
离子束溅射技术是制备Ta2O5薄膜的重要技术之一。采用正交试验设计方法,系统研究了Ta2O5薄膜的折射率、折射率非均匀性、消光系数、沉积速率和应力与工艺参数(基板温度、离子束压、离子束流和氧气流量)之间的关联性。通过使用分光光度计和椭圆偏振仪测量Ta2O5薄膜透过率光谱和反射椭偏特性,再利用全光谱反演计算的方法获得薄膜的折射率、折射率非均匀性、消光系数和物理厚度。Ta2O5薄膜的应力通过测量基底镀膜前后的表面变形量计算得到。实验结果表明:基板温度是影响Ta2O5薄膜特性的共性关键要素,其他工艺参数的选择与需求的薄膜特性相关。研究结果对于制备不同应用的Ta2O5薄膜制备工艺参数选择具有指导意义。
離子束濺射技術是製備Ta2O5薄膜的重要技術之一。採用正交試驗設計方法,繫統研究瞭Ta2O5薄膜的摺射率、摺射率非均勻性、消光繫數、沉積速率和應力與工藝參數(基闆溫度、離子束壓、離子束流和氧氣流量)之間的關聯性。通過使用分光光度計和橢圓偏振儀測量Ta2O5薄膜透過率光譜和反射橢偏特性,再利用全光譜反縯計算的方法穫得薄膜的摺射率、摺射率非均勻性、消光繫數和物理厚度。Ta2O5薄膜的應力通過測量基底鍍膜前後的錶麵變形量計算得到。實驗結果錶明:基闆溫度是影響Ta2O5薄膜特性的共性關鍵要素,其他工藝參數的選擇與需求的薄膜特性相關。研究結果對于製備不同應用的Ta2O5薄膜製備工藝參數選擇具有指導意義。
리자속천사기술시제비Ta2O5박막적중요기술지일。채용정교시험설계방법,계통연구료Ta2O5박막적절사솔、절사솔비균균성、소광계수、침적속솔화응력여공예삼수(기판온도、리자속압、리자속류화양기류량)지간적관련성。통과사용분광광도계화타원편진의측량Ta2O5박막투과솔광보화반사타편특성,재이용전광보반연계산적방법획득박막적절사솔、절사솔비균균성、소광계수화물리후도。Ta2O5박막적응력통과측량기저도막전후적표면변형량계산득도。실험결과표명:기판온도시영향Ta2O5박막특성적공성관건요소,기타공예삼수적선택여수구적박막특성상관。연구결과대우제비불동응용적Ta2O5박막제비공예삼수선택구유지도의의。
Ion beam sputtering is one of the best important technologies for preparing Ta2O5 thin films. The correlation properties of Ta2O5 thin films and preparative parameters (substrate temperature, ion beam voltage, ion beam current and oxygen flow) were systemic researched by using the orthogonal experiment design method. The Ta2O5 thin films properties (refractive index, extinction coefficient, deposition rate, stress and inhomogeneity of refractive index) were studied. The refractive index, extinction coefficient, physical thickness and inhomogeneity of refractive index were measured by multiple wavelength curve-fitting method from the reflectance and transmittance of samples. The stress of thin film was measured by elastic deformation of thin film-substrate system. An experimental design strategy used substrate temperature, ion beam voltage, ion beam current, and oxygen flow as the variables. The experimental results indicate that the temperature of substrate is key influence parameter on Ta2O5 thin films properties and other preparative parameters are correlation with specific thin films properties. The results can be used to select the proper preparative parameters for preparing Ta2O5 thin films with different applications.