CAJ | 학술논문

建立高效液相色谱仪自动进样器的校准方法，并对其测量不确定度进行评定。参考欧洲医药管理局《质量控制文件》提供的方法对液相色谱仪自动进样器的进样体积误差、进样残留和进样重复性建立校准方法，经评定得进样体积误差的相对扩展不确定度为1.8%。高效液相色谱仪自动进样器校准方法及不确定度评定方法的建立，为高效液相色谱仪自动进样器的校准提供依据。
건립고효액상색보의자동진양기적교준방법，병대기측량불학정도진행평정。삼고구주의약관리국《질량공제문건》제공적방법대액상색보의자동진양기적진양체적오차、진양잔류화진양중복성건립교준방법，경평정득진양체적오차적상대확전불학정도위1.8%。고효액상색보의자동진양기교준방법급불학정도평정방법적건립，위고효액상색보의자동진양기적교준제공의거。
HPLC auto-sampler calibration method was established and its measurement uncertainty was evaluated. The method of HPLC auto-sampler injection volume error, injection build residual, and repeatability calibration method was established through the reference of the european medicines authority Quality Control Document, and the error injection volume relative expanded uncertainty degree was calculated of 1.8%. The establishment calibration methods and uncertainty evaluation provided the basis for calibration of HPLC auto-sampler.