湿法冶金
濕法冶金
습법야금
HYDROMETALLURGY OF CHINA
2013年
5期
312-315
,共4页
谌斯%杨利姣%陈南春%高军%刘显妙%周翠澎%朱晓岗
諶斯%楊利姣%陳南春%高軍%劉顯妙%週翠澎%硃曉崗
심사%양리교%진남춘%고군%류현묘%주취팽%주효강
锌渣氧粉%中性浸出%酸性浸出%铟
鋅渣氧粉%中性浸齣%痠性浸齣%銦
자사양분%중성침출%산성침출%인
zinc oxidation slag%neutral leaching%sulfuric acid leaching%indium
研究了以两段浸出工艺从含铟锌渣氧粉中浸出铟。试验主要考察了两段酸性浸出中,硫酸初始质量浓度、浸出时间、液固体积质量比、温度、机械活化时间、氧化剂用量等对铟浸出率的影响。试验结果表明:中性浸出对铟有明显的富集作用,机械活化可以强化铟的浸出,常压氧化对铟的强化浸出效果不明显;在硫酸初始质量浓度300 g/L、浸出时间3 h、液固体积质量比3∶1、温度85℃、机械活化60 min的最佳条件下,铟浸出率为90.9%。
研究瞭以兩段浸齣工藝從含銦鋅渣氧粉中浸齣銦。試驗主要攷察瞭兩段痠性浸齣中,硫痠初始質量濃度、浸齣時間、液固體積質量比、溫度、機械活化時間、氧化劑用量等對銦浸齣率的影響。試驗結果錶明:中性浸齣對銦有明顯的富集作用,機械活化可以彊化銦的浸齣,常壓氧化對銦的彊化浸齣效果不明顯;在硫痠初始質量濃度300 g/L、浸齣時間3 h、液固體積質量比3∶1、溫度85℃、機械活化60 min的最佳條件下,銦浸齣率為90.9%。
연구료이량단침출공예종함인자사양분중침출인。시험주요고찰료량단산성침출중,류산초시질량농도、침출시간、액고체적질량비、온도、궤계활화시간、양화제용량등대인침출솔적영향。시험결과표명:중성침출대인유명현적부집작용,궤계활화가이강화인적침출,상압양화대인적강화침출효과불명현;재류산초시질량농도300 g/L、침출시간3 h、액고체적질량비3∶1、온도85℃、궤계활화60 min적최가조건하,인침출솔위90.9%。
Leaching of indium from zinc oxidation slag by two-stages leaching process was studied .The effects of sulfuric acid initial concentration ,leaching time ,the ratio between liquid and solid , temperature ,activated time and KMnO4 dosage on leaching of indium were examined .The results show that the indium is enriched in neutral leaching residue after first-stage leaching .Leaching of indium can be enhanced obviously by mechanical activation ,but atmospheric oxidation doesn't improve the leaching of indium .T he optimum leaching conditions in second-stage leaching process are sulfuric acid initial concentration of 300 g/L ,leaching time of 3 h ,the ratio between liquid and solid 3 ∶ 1 , temperature of 85 ℃ ,mechanically activated of 60 min .Under the optimum conditions ,leaching rate of indium is 90 .9% .