CAJ | 학술논문

目的对鼻炎合剂进行定性定量分析。方法采用薄层色谱法对鼻炎合剂中桔梗、桑叶、辛夷进行定性鉴别；以绿原酸为指标成分，采用高效液相色谱法对其进行定量分析。结果各薄层定性色谱中，在与对照药材相应的位置上显相同颜色的斑点，阴性对照未见干扰；绿原酸在0.1072～0.8936μg范围内呈现良好的线性关系，r≈0.999997，平均加样回收率为99.05%。结论定性定量方法简单，重复性好，结果准确，可用于鼻炎合剂的质量控制。
목적대비염합제진행정성정량분석。방법채용박층색보법대비염합제중길경、상협、신이진행정성감별；이록원산위지표성분，채용고효액상색보법대기진행정량분석。결과각박층정성색보중，재여대조약재상응적위치상현상동안색적반점，음성대조미견간우；록원산재0.1072～0.8936μg범위내정현량호적선성관계，r≈0.999997，평균가양회수솔위99.05%。결론정성정량방법간단，중복성호，결과준학，가용우비염합제적질량공제。
Objective To analyse the quality of Biyan Mixture. Methods Platycodonis Radix, Mori Folium and Magnoliae Flos in the preparation were identified by TLC, and the content of chlorogenic acid was determined by HPLC. Results Among all the methods of the TLC, the contrapositive drug ingredients had the same tinctorial spot in the corresponding position, and there were no interference in the negative constrast. The linear range of chlorogenic acid was 0.1072~0.8936 μg, r≈0.999997. The average recovery was 99.05 %. Conclusion The methods were simple, reliable and accurate. It could be applied to the quality control of Biyan Mixture.