中国有色金属学报
中國有色金屬學報
중국유색금속학보
THE CHINESE JOURNAL OF NONFERROUS METALS
2013年
10期
2846-2850
,共5页
秦丽元%连建设%蒋恩臣%刘中原
秦麗元%連建設%蔣恩臣%劉中原
진려원%련건설%장은신%류중원
镍钴合金%电沉积%纳米晶%双相结构%力学性能
鎳鈷閤金%電沉積%納米晶%雙相結構%力學性能
얼고합금%전침적%납미정%쌍상결구%역학성능
Ni-Co alloy%electrodeposition%nanocrystalline%dual-phase microstructure%mechanical property
采用直流电沉积方法制备晶粒尺寸为15 nm的Ni-49.2%Co(质量分数)和16 nm的Ni-66.7%Co(质量分数)合金。采用XRD、TEM和MTS?810万能材料试验机对其微观结构和力学性能进行分析。结果表明:两种合金分别是单相FCC结构和FCC与HCP共存的双相结构。固溶强化和晶粒细化的作用使两种Ni-Co合金都具有很高的抗拉强度;且Co元素的引入降低材料的层错能,提高其应变硬化能力,使Ni-Co合金的塑性也明显提高;Ni-49.2%Co合金的抗拉强度(σb )和断裂伸长率(δ)分别为1650 MPa和9%,Ni-66.7%Co合金的σb和δ分别为2200 MPa和12%。Ni-66.7%Co合金中FCC和HCP结构相互协调,在变形过程中释放内应力,使材料应变硬化能力得以保持,所以获得更高的强度和塑性。
採用直流電沉積方法製備晶粒呎吋為15 nm的Ni-49.2%Co(質量分數)和16 nm的Ni-66.7%Co(質量分數)閤金。採用XRD、TEM和MTS?810萬能材料試驗機對其微觀結構和力學性能進行分析。結果錶明:兩種閤金分彆是單相FCC結構和FCC與HCP共存的雙相結構。固溶彊化和晶粒細化的作用使兩種Ni-Co閤金都具有很高的抗拉彊度;且Co元素的引入降低材料的層錯能,提高其應變硬化能力,使Ni-Co閤金的塑性也明顯提高;Ni-49.2%Co閤金的抗拉彊度(σb )和斷裂伸長率(δ)分彆為1650 MPa和9%,Ni-66.7%Co閤金的σb和δ分彆為2200 MPa和12%。Ni-66.7%Co閤金中FCC和HCP結構相互協調,在變形過程中釋放內應力,使材料應變硬化能力得以保持,所以穫得更高的彊度和塑性。
채용직류전침적방법제비정립척촌위15 nm적Ni-49.2%Co(질량분수)화16 nm적Ni-66.7%Co(질량분수)합금。채용XRD、TEM화MTS?810만능재료시험궤대기미관결구화역학성능진행분석。결과표명:량충합금분별시단상FCC결구화FCC여HCP공존적쌍상결구。고용강화화정립세화적작용사량충Ni-Co합금도구유흔고적항랍강도;차Co원소적인입강저재료적층착능,제고기응변경화능력,사Ni-Co합금적소성야명현제고;Ni-49.2%Co합금적항랍강도(σb )화단렬신장솔(δ)분별위1650 MPa화9%,Ni-66.7%Co합금적σb화δ분별위2200 MPa화12%。Ni-66.7%Co합금중FCC화HCP결구상호협조,재변형과정중석방내응력,사재료응변경화능력득이보지,소이획득경고적강도화소성。
Nanocrystalline Ni-49.2%Co (mass fraction) and Ni-66.7%Co (mass fraction) alloys were synthesized by direct current electrodeposition with grain sizes of 15 and 16 nm, respectively. The Ni-49.2%Co alloy shows single FCC phase, and Ni-66.7%Co alloy possesses a mixture structure of FCC and HCP phase. The microstructure and mechanical properties of were studied by XRD, TEM and tensile tests carried out on MTS?810 tester. The high strength of Ni-Co alloys is attributed to the grain refinement and solid-solution hardening effects. The addition of Co element decreases the stacking fault energy of nanocrystalline Ni alloy, which improves the strain hardening ability and thus enhances the ductility. The ultimate tensile strength (σb ) and elongation to failure (δ) of Ni-49.2%Co alloy are 1 650 MPa and 9%, respectively. Correspondingly, the σb and δ of Ni-66.7%Co alloy are 2 200 MPa and 12%, respectively. Cooperative deformation of the two phases releases the stress during deformation effectively, which contributes to the sustained high strain hardening and ductility of the Ni-66.7%Co alloy.