河南科学
河南科學
하남과학
HENAN SCIENCE
2013年
9期
1358-1361
,共4页
姜垒%付阳%霍萃萌%李岩%任志勇
薑壘%付暘%霍萃萌%李巖%任誌勇
강루%부양%곽췌맹%리암%임지용
桐油%二乙醇胺%胺解
桐油%二乙醇胺%胺解
동유%이을순알%알해
Tung oil%diethanolamine%aminolysis
利用二乙醇胺和桐油进行胺解反应，成功地制备了主要含有两个羟基的桐油多元醇。考察了本体聚合工艺条件（引发剂浓度、单体配比、聚合温度、聚合时间）对胺解转化率的影响，利用液相、红外光谱对所得产物结构进行了表征。
利用二乙醇胺和桐油進行胺解反應，成功地製備瞭主要含有兩箇羥基的桐油多元醇。攷察瞭本體聚閤工藝條件（引髮劑濃度、單體配比、聚閤溫度、聚閤時間）對胺解轉化率的影響，利用液相、紅外光譜對所得產物結構進行瞭錶徵。
이용이을순알화동유진행알해반응，성공지제비료주요함유량개간기적동유다원순。고찰료본체취합공예조건（인발제농도、단체배비、취합온도、취합시간）대알해전화솔적영향，이용액상、홍외광보대소득산물결구진행료표정。
In the present paper,Tung oil polyols with conjugated double bonds were prepared through aminolysis by diethanolamine. FTIR and liquid chromatograph were used to characterize their structures. The effects of the mixing ratio of monomers,the initiator concentration,the polymerization temperature and time on the reaction conversion rate were also discussed. The results confirmed the structure of Tung oil polyols and obtained the preferential synthesis process.
