电镀与涂饰
電鍍與塗飾
전도여도식
ELECTROPLATING & FINISHING
2014年
9期
366-368
,共3页
锌铝复合镀层%湿法机械镀%超声振动%形貌%厚度%结合力
鋅鋁複閤鍍層%濕法機械鍍%超聲振動%形貌%厚度%結閤力
자려복합도층%습법궤계도%초성진동%형모%후도%결합력
zinc-aluminum composite coating%wet mechanical plating%ultrasonic vibration%morphology%thickness%adhesion
以 Q235钢片为基体,采用湿法超声机械镀制备 Zn-Al复合镀层。用扫描电子显微镜及其配备的能谱仪分析了锌-铝复合镀层的表面形貌、断面形貌和元素组成,并用测厚仪、贴滤纸法和划格试验分别对镀层的厚度、孔隙率和结合力进行表征。结果表明,湿法超声机械镀Zn-Al复合镀层是由锌粉和铝粉颗粒相互镶嵌、填充所形成的致密堆积体,表面均匀、平整,与基体的结合强度高。镀层主要由锌、铝、锡和铁组成,铝的质量分数低于施镀前混合粉体中铝粉的质量分数。在考虑施镀过程中金属粉的损耗后,所得Zn-Al镀层的厚度满足预定的厚度(30μm)要求。
以 Q235鋼片為基體,採用濕法超聲機械鍍製備 Zn-Al複閤鍍層。用掃描電子顯微鏡及其配備的能譜儀分析瞭鋅-鋁複閤鍍層的錶麵形貌、斷麵形貌和元素組成,併用測厚儀、貼濾紙法和劃格試驗分彆對鍍層的厚度、孔隙率和結閤力進行錶徵。結果錶明,濕法超聲機械鍍Zn-Al複閤鍍層是由鋅粉和鋁粉顆粒相互鑲嵌、填充所形成的緻密堆積體,錶麵均勻、平整,與基體的結閤彊度高。鍍層主要由鋅、鋁、錫和鐵組成,鋁的質量分數低于施鍍前混閤粉體中鋁粉的質量分數。在攷慮施鍍過程中金屬粉的損耗後,所得Zn-Al鍍層的厚度滿足預定的厚度(30μm)要求。
이 Q235강편위기체,채용습법초성궤계도제비 Zn-Al복합도층。용소묘전자현미경급기배비적능보의분석료자-려복합도층적표면형모、단면형모화원소조성,병용측후의、첩려지법화화격시험분별대도층적후도、공극솔화결합력진행표정。결과표명,습법초성궤계도Zn-Al복합도층시유자분화려분과립상호양감、전충소형성적치밀퇴적체,표면균균、평정,여기체적결합강도고。도층주요유자、려、석화철조성,려적질량분수저우시도전혼합분체중려분적질량분수。재고필시도과정중금속분적손모후,소득Zn-Al도층적후도만족예정적후도(30μm)요구。
Zn–Al composite coating was prepared on Q235 steel substrate by ultrasonic-based wet mechanical plating. The surface morphology, cross-sectional morphology, and elemental composition of the coating were analyzed by scanning electron microscopy and energy-dispersive spectroscopy. The thickness, porosity, and adhesion strength of the coating were characterized using thickness tester, ferroxyl test, and cross-cut test, respectively. The results showed that the Zn–Al composite coating prepared by ultrasonic-based wet mechanical plating is a compact stacked layer mutually inlaid and filled by zinc and aluminum particles, with uniform and smooth surface and strong adhesion to the substrate. The Zn–Al coating consists mainly of zinc, aluminum, tin, and iron. The mass fraction of aluminum in the coating is lower than that of aluminum in the particle mixture before plating. The thickness of Zn–Al coating reaches the expected value (30μm) after considering the loss of metal particles during the plating process.