CAJ | 학술논문

氧代异佛尔酮(KIP)是合成维生素E的重要中间体，目前主要有两条合成路线。本文研究了以α-异佛尔酮为原料，在催化体系作用下，用分子氧氧化制备氧代异佛尔酮的合成工艺。同时采用喷射氧化反应，验证了催化剂用量、反应温度、氧含量等因素对收率的影响。
양대이불이동(KIP)시합성유생소E적중요중간체，목전주요유량조합성로선。본문연구료이α-이불이동위원료，재최화체계작용하，용분자양양화제비양대이불이동적합성공예。동시채용분사양화반응，험증료최화제용량、반응온도、양함량등인소대수솔적영향。
Ketoisophorone (KIP)is an important intermediate of vitamin E. Currently, there are two syn-thetic routes to get KIP. This paper studies the direct oxidation of α-isophorone to KIP by dioxygen in catalytic system. At the same time,use the jet oxidation reaction. The effect on yield was studied including catalyst quantity, temperature,dissolved oxygen.