黑龙江医药
黑龍江醫藥
흑룡강의약
HEILONGJIANG MEDICAL JOURNAL
2013年
5期
762-764,765
,共4页
桑寄生%威灵仙%粉防已碱%双波长薄层扫描法
桑寄生%威靈仙%粉防已堿%雙波長薄層掃描法
상기생%위령선%분방이감%쌍파장박층소묘법
Herba Tzxilli%Radix Clematidis%Tetrandrine%Dual wavelength thin layer chromatography scanning
目的：建立莶风湿片的质量可控标准。方法：采用TLC对药品中桑寄生、威灵仙的成分进行色谱鉴别，并采用双波长薄层扫描法测定防已药材中粉防已碱的含量。结果：分别以桑寄生、威灵仙对照药材为对照，建立了薄层鉴别方法。并规定本品含防已以粉防己碱计不得少于0.60mg/片。粉防已碱在0.51~2.55μg范围内呈较好的线性关系，回收率为96.68%， RSD为1.96%。结论：本质量标准可有效的控制莶风湿片的质量
目的：建立薟風濕片的質量可控標準。方法：採用TLC對藥品中桑寄生、威靈仙的成分進行色譜鑒彆，併採用雙波長薄層掃描法測定防已藥材中粉防已堿的含量。結果：分彆以桑寄生、威靈仙對照藥材為對照，建立瞭薄層鑒彆方法。併規定本品含防已以粉防己堿計不得少于0.60mg/片。粉防已堿在0.51~2.55μg範圍內呈較好的線性關繫，迴收率為96.68%， RSD為1.96%。結論：本質量標準可有效的控製薟風濕片的質量
목적：건립렴풍습편적질량가공표준。방법：채용TLC대약품중상기생、위령선적성분진행색보감별，병채용쌍파장박층소묘법측정방이약재중분방이감적함량。결과：분별이상기생、위령선대조약재위대조，건립료박층감별방법。병규정본품함방이이분방기감계불득소우0.60mg/편。분방이감재0.51~2.55μg범위내정교호적선성관계，회수솔위96.68%， RSD위1.96%。결론：본질량표준가유효적공제렴풍습편적질량
Objective: Ob jective:To establish the quality standard of Xixianfengshi tablet.Methods:Herba Taxilli,Rsdix Clematidis in xilianfengshi tablet were identified by thin-layer chromatography.The contents of tetrandrune in Rradix Stephaniae Tetrandrac were quantitatively determined by double-wavelength TLC scanning.Results:The two traditional Chinese herbs in xixianfengshi tablet,llerba Taxilli and Radix Clematidis,were qualitaivly identified by TLC methods And ruled Radix Stephaniae Tetrandrae in the Xixianfengshi pian to account with the Tetrandrine cannot less than 0.6mg/slice.The standard curve was lin-ear in the rage of 0.51-2.55μg for Tetrandrine,the recovery of Tetrandring was 96.68% and RSD was 1.96%.Conclusion:This standard is capable to effectively control the quality of Xixianfengshi tablet.
