光谱学与光谱分析
光譜學與光譜分析
광보학여광보분석
SPECTROSCOPY AND SPECTRAL ANALYSIS
2013年
11期
3002-3009
,共8页
陶琳丽%杨秀娟%邓君明%张曦
陶琳麗%楊秀娟%鄧君明%張晞
도림려%양수연%산군명%장희
近红外光谱检测技术%肉%化学成分%综述
近紅外光譜檢測技術%肉%化學成分%綜述
근홍외광보검측기술%육%화학성분%종술
Near infrared reflectance spectroscopy (NIRS)%Meat%Chemical compositions%Review
和传统的肉品化学成分检测方法相比,近红外光谱分析是一种能够快速、简单、安全和可同时测定多种化学成分的肉品检测方法。论述了近年来猪、鸡、牛、羊四种动物肉中粗蛋白质、肌间脂肪、脂肪酸、水分、灰分、肌红蛋白和胶原蛋白七种化学成分的近红外光谱分析检测研究进展,并探讨了目前研究中存在的问题及其原因。从已发表的研究结果可以看出,近红外光谱分析具有替代耗时成本高的现有肉品化学检测方法的巨大潜力,特别是用于商业上同步检测多种化学成分。研究大多采用主成分分析法进行特征光谱筛选,偏最小二乘和修正偏最小二乘法建立校正模型,交互验证进行预测结果评价。目前研究热点集中在肉中脂肪酸含量预测模型和应用近红外高光谱图像和多元回归预测肉中化学成分。近红外光谱预测结果差异性较大,这与样品集选择、光谱预处理和建模方法都有很密切的关系。样品选择对近红外预测精度具有重要的意义,非均质肉样影响了近红外化学成分预测精度。总的来说,肌间脂肪、脂肪酸与水分指标预测效果较好,粗蛋白质和肌红蛋白指标预测效果次之,灰分和胶原蛋白指标预测结果较差。
和傳統的肉品化學成分檢測方法相比,近紅外光譜分析是一種能夠快速、簡單、安全和可同時測定多種化學成分的肉品檢測方法。論述瞭近年來豬、鷄、牛、羊四種動物肉中粗蛋白質、肌間脂肪、脂肪痠、水分、灰分、肌紅蛋白和膠原蛋白七種化學成分的近紅外光譜分析檢測研究進展,併探討瞭目前研究中存在的問題及其原因。從已髮錶的研究結果可以看齣,近紅外光譜分析具有替代耗時成本高的現有肉品化學檢測方法的巨大潛力,特彆是用于商業上同步檢測多種化學成分。研究大多採用主成分分析法進行特徵光譜篩選,偏最小二乘和脩正偏最小二乘法建立校正模型,交互驗證進行預測結果評價。目前研究熱點集中在肉中脂肪痠含量預測模型和應用近紅外高光譜圖像和多元迴歸預測肉中化學成分。近紅外光譜預測結果差異性較大,這與樣品集選擇、光譜預處理和建模方法都有很密切的關繫。樣品選擇對近紅外預測精度具有重要的意義,非均質肉樣影響瞭近紅外化學成分預測精度。總的來說,肌間脂肪、脂肪痠與水分指標預測效果較好,粗蛋白質和肌紅蛋白指標預測效果次之,灰分和膠原蛋白指標預測結果較差。
화전통적육품화학성분검측방법상비,근홍외광보분석시일충능구쾌속、간단、안전화가동시측정다충화학성분적육품검측방법。논술료근년래저、계、우、양사충동물육중조단백질、기간지방、지방산、수분、회분、기홍단백화효원단백칠충화학성분적근홍외광보분석검측연구진전,병탐토료목전연구중존재적문제급기원인。종이발표적연구결과가이간출,근홍외광보분석구유체대모시성본고적현유육품화학검측방법적거대잠력,특별시용우상업상동보검측다충화학성분。연구대다채용주성분분석법진행특정광보사선,편최소이승화수정편최소이승법건립교정모형,교호험증진행예측결과평개。목전연구열점집중재육중지방산함량예측모형화응용근홍외고광보도상화다원회귀예측육중화학성분。근홍외광보예측결과차이성교대,저여양품집선택、광보예처리화건모방법도유흔밀절적관계。양품선택대근홍외예측정도구유중요적의의,비균질육양영향료근홍외화학성분예측정도。총적래설,기간지방、지방산여수분지표예측효과교호,조단백질화기홍단백지표예측효과차지,회분화효원단백지표예측결과교차。
In contrast to conventional methods for the determination of meat chemical composition ,near infrared reflectance spec-troscopy enables rapid ,simple ,secure and simultaneous assessment of numerous meat properties .The present review focuses on the use of near infrared reflectance spectroscopy to predict meat chemical compositions .The potential of near infrared reflectance spectroscopy to predict crude protein ,intramuscular fat ,fatty acid ,moisture ,ash ,myoglobin and collagen of beef ,pork ,chick-en and lamb is reviewed .This paper discusses existing questions and reasons in the current research .According to the published results ,although published results vary considerably ,they suggest that near-infrared reflectance spectroscopy shows a great po-tential to replace the expensive and time-consuming chemical analysis of meat composition .In particular ,under commercial con-ditions where simultaneous measurements of different chemical components are required ,near infrared reflectance spectroscopy is expected to be the method of choice .The majority of studies selected feature-related wavelengths using principal components re-gression ,developed the calibration model using partial least squares and modified partial least squares ,and estimated the predic-tion accuracy by means of cross-validation using the same sample set previously used for the calibration .Meat fatty acid composi-tion predicted by near-infrared spectroscopy and non-destructive prediction and visualization of chemical composition in meat u-sing near-infrared hyperspectral imaging and multivariate regression are the hot studying field now .On the other hand ,near in-frared reflectance spectroscopy shows great difference for predicting different attributes of meat quality which are closely related to the selection of calibration sample set ,preprocessing of near-infrared spectroscopy and modeling approach .Sample preparation also has an important effect on the reliability of NIR prediction ;in particular ,lack of homogeneity of the meat samples influenced the accuracy of estimation of chemical components .In general the predicting results of intramuscular fat ,fatty acid and moisture are best ,the predicting results of crude protein and myoglobin are better ,while the predicting results of ash and collagen are less accurate .