北方药学
北方藥學
북방약학
JOURNAL OF NORTH PHARMACY
2013年
11期
1-2
,共2页
霍文杰%高英%李卫民%朱贺年
霍文傑%高英%李衛民%硃賀年
곽문걸%고영%리위민%주하년
甘草%富集%异戊烯基黄酮%高效液相色谱-质谱联用
甘草%富集%異戊烯基黃酮%高效液相色譜-質譜聯用
감초%부집%이무희기황동%고효액상색보-질보련용
Licorice%Enrichment%Prenylated flavonoids%HPLC-MS
目的:对甘草中异戊烯基类黄酮部位的富集工艺研究及色谱峰定性分析,了解甘草中异戊烯基类黄酮的化学成分。方法:以浸膏得率及总黄酮含量为衡量指标,对甘草中的异戊烯基类黄酮进行富集;通过高效液相色谱-质谱联用法对甘草中异戊烯基类黄酮进行分析。结果:结合文献对图谱的色谱峰进行鉴定,推断出具异戊烯基基团的黄酮有23种,确定化学结构的有12种。为下一步甘草异戊烯基类黄酮部位研究打下了基础。
目的:對甘草中異戊烯基類黃酮部位的富集工藝研究及色譜峰定性分析,瞭解甘草中異戊烯基類黃酮的化學成分。方法:以浸膏得率及總黃酮含量為衡量指標,對甘草中的異戊烯基類黃酮進行富集;通過高效液相色譜-質譜聯用法對甘草中異戊烯基類黃酮進行分析。結果:結閤文獻對圖譜的色譜峰進行鑒定,推斷齣具異戊烯基基糰的黃酮有23種,確定化學結構的有12種。為下一步甘草異戊烯基類黃酮部位研究打下瞭基礎。
목적:대감초중이무희기류황동부위적부집공예연구급색보봉정성분석,료해감초중이무희기류황동적화학성분。방법:이침고득솔급총황동함량위형량지표,대감초중적이무희기류황동진행부집;통과고효액상색보-질보련용법대감초중이무희기류황동진행분석。결과:결합문헌대도보적색보봉진행감정,추단출구이무희기기단적황동유23충,학정화학결구적유12충。위하일보감초이무희기류황동부위연구타하료기출。
Objective:To study the enrichment of prenylated flavonoids of licorice and identify the constituents of prenylated flavonoids of licorice in methanol extract. Methods:Extraction rate and Total flavonoids were used as indexes to determine the enrichment, HPLC-MS of methanol extract of licorice were analized. Results:Peaks were identified combined with literature data, and 23 probable compounds were inferred.