CAJ | 학술논문

目的：建立紫朱软膏的质量标准。方法采用薄层色谱法对紫朱软膏中的紫草、冰片进行鉴别,采用气相色谱法测定制剂中冰片的含量。结果薄层色谱中主斑点清晰,分离度好；冰片在0.0484～1.2100μg范围内线性关系良好,加样回收率在90%～110%范围内,RSD＜5%。结论本方法简便可行,可用于紫朱软膏的质量控制。
목적：건립자주연고적질량표준。방법채용박층색보법대자주연고중적자초、빙편진행감별,채용기상색보법측정제제중빙편적함량。결과박층색보중주반점청석,분리도호；빙편재0.0484～1.2100μg범위내선성관계량호,가양회수솔재90%～110%범위내,RSD＜5%。결론본방법간편가행,가용우자주연고적질량공제。
Objective To establish the quality standards of Zizhu ointment. Methods The TLC was applied to identify Radix arnebiae and borneol of Zizhu ointment, and the content of borneol was determined by gas chromatography. Results The TLC spots were clear, well-separated and easy to identify. The good linear range of borneol reference substance on calibration curve was 0.048 4-1.210 0 μg, and the recovery was 90%-110%, the relative standard deviation was less than 5%. Conclusion The method is simple and feasible, can be used as the quality control method of Zizhu ointment.