江西中医药大学学报
江西中醫藥大學學報
강서중의약대학학보
Journal of Jiangxi University of Traditional Chinese Medicine
2014年
3期
55-57
,共3页
万江%何平清%何纯斌%杨明%张明明
萬江%何平清%何純斌%楊明%張明明
만강%하평청%하순빈%양명%장명명
三味檀香口服液%正交设计%原儿茶酸
三味檀香口服液%正交設計%原兒茶痠
삼미단향구복액%정교설계%원인다산
Sanwei Tanxiang%Oral Solution%orthogonal design%3,4-Dihydroxybenzoic acid
目的：研究三味檀香口服液制备的最佳工艺。方法：选用L9（34）进行正交设计实验，对三味檀香口服液的提取工艺进行优选，以原儿茶酸含量为指标，考察乙醇浓度，乙醇用量和回流时间3个因素。结果：乙醇浓度为70％，6倍量回流2次，每次2小时，提取效果最好。结论：该工艺稳定可靠，适合工业化大生产。
目的：研究三味檀香口服液製備的最佳工藝。方法：選用L9（34）進行正交設計實驗，對三味檀香口服液的提取工藝進行優選，以原兒茶痠含量為指標，攷察乙醇濃度，乙醇用量和迴流時間3箇因素。結果：乙醇濃度為70％，6倍量迴流2次，每次2小時，提取效果最好。結論：該工藝穩定可靠，適閤工業化大生產。
목적：연구삼미단향구복액제비적최가공예。방법：선용L9（34）진행정교설계실험，대삼미단향구복액적제취공예진행우선，이원인다산함량위지표，고찰을순농도，을순용량화회류시간3개인소。결과：을순농도위70％，6배량회류2차，매차2소시，제취효과최호。결론：해공예은정가고，괄합공업화대생산。
Objective:To study the factor which had effect on the prepration technology of Sanwei Tanxiang Oral Solution , to Select the best preparation conditons .Methods:By determining 3,4-Dihydroxybenzoic acid in extract ,the process was optimized with orthogonal design with 3 factors and 3 levels.Employing the content of 3,4-Dihydroxybenzoic acid , the effect of refluxing time ,ethanol concen-tration and ratio of material to liquid .Results:The optimum extraction conditions were 6 folds of 70%ethanol ,refluxing 2 h,extracting 2 times.Conclusion:The process was stable and reliable , easy and available , suitable for manufacturing of Sanwei Tanxiang Oral So-lution.
