功能材料
功能材料
공능재료
JOURNAL OF FUNCTIONAL MATERIALS
2014年
z1期
165-168
,共4页
常敬先%李海蓉%马国富%王鹏
常敬先%李海蓉%馬國富%王鵬
상경선%리해용%마국부%왕붕
SOI%铜膜生长法%前驱体%热处理%CuO 纳米线
SOI%銅膜生長法%前驅體%熱處理%CuO 納米線
SOI%동막생장법%전구체%열처리%CuO 납미선
SOI%the copper film growth method%precursor%thermal annealing%CuO nanowires
在SOI基上制备光电纳米器件具有良好的光电集成应用前景,通过铜膜生长法在 SOI 基上制备了形貌为类针状的 Cu(OH)2前驱体纳米线,并采用热处理法600℃条件下成功制备了 CuO 纳米线。通过扫描电镜(SEM)、透射电镜(TEM)、X 射线衍射测试(XRD)对样品结构、形貌进行了表征。 SEM、TEM测试结果表明,Cu(OH)2前驱体纳米线结构一致,尺寸均匀,表面光滑。在 Cu(OH)2前驱体纳米线上二次生长的CuO 纳米线具有类蒲草状细长光滑的结构, CuO纳米线直径约为80~100 nm,长度约为10μm, CuO 纳米线结晶性良好。
在SOI基上製備光電納米器件具有良好的光電集成應用前景,通過銅膜生長法在 SOI 基上製備瞭形貌為類針狀的 Cu(OH)2前驅體納米線,併採用熱處理法600℃條件下成功製備瞭 CuO 納米線。通過掃描電鏡(SEM)、透射電鏡(TEM)、X 射線衍射測試(XRD)對樣品結構、形貌進行瞭錶徵。 SEM、TEM測試結果錶明,Cu(OH)2前驅體納米線結構一緻,呎吋均勻,錶麵光滑。在 Cu(OH)2前驅體納米線上二次生長的CuO 納米線具有類蒲草狀細長光滑的結構, CuO納米線直徑約為80~100 nm,長度約為10μm, CuO 納米線結晶性良好。
재SOI기상제비광전납미기건구유량호적광전집성응용전경,통과동막생장법재 SOI 기상제비료형모위류침상적 Cu(OH)2전구체납미선,병채용열처리법600℃조건하성공제비료 CuO 납미선。통과소묘전경(SEM)、투사전경(TEM)、X 사선연사측시(XRD)대양품결구、형모진행료표정。 SEM、TEM측시결과표명,Cu(OH)2전구체납미선결구일치,척촌균균,표면광활。재 Cu(OH)2전구체납미선상이차생장적CuO 납미선구유류포초상세장광활적결구, CuO납미선직경약위80~100 nm,장도약위10μm, CuO 납미선결정성량호。
Preparation of optoelectronic nanodevices on SOI substrate has good prospects in optoelectronic inte-grated applications.CuO nanowires have been successfully prepared on the SOI substrate at 600 ℃ by the heat treatment method of Cu(OH)2 precursors nanowires,which were pre-prepared by the copper film growth meth-od.Morphology and structures of the samples were characterized by scanning electron microscope (SEM), transmission electron microscopy (TEM),and X-ray diffraction (XRD).The SEM and TEM testing results showed that Cu(OH)2 precursors nanowires were needle-like with consistent structure and smooth and uniform surface.The CuO nanowires were cattail-like with tenuous and smooth structure.The diameter of CuO nanowires was about 80-100 nm,the length of nanowires was about 10μm.A good crystalline quality of CuO nanowires were obtained.