化学分析计量
化學分析計量
화학분석계량
CHEMICAL ANALYSIS AND METERAGE
2014年
2期
30-34
,共5页
柏婷%伊奥尔%汤建国%祝琳华%乔丹娜%孟昭宇
柏婷%伊奧爾%湯建國%祝琳華%喬丹娜%孟昭宇
백정%이오이%탕건국%축림화%교단나%맹소우
烟草%酶解%果胶%离子色谱%果胶酶
煙草%酶解%果膠%離子色譜%果膠酶
연초%매해%과효%리자색보%과효매
tobacco%enzymolysis%pectin%ion chromatography%pectinase
为了提高YC/T 346-2010果胶含量测定方法的分析速度,将标准中醇化除糖、滤渣酸化两步前处理优化为一步,即酸醇溶液加热回流同时除糖和酸化,并将方法改进前后的测定结果进行比较分析。一步前处理方法线性相关系数为0.9999,回收率为93.57%~102.29%,测定结果的相对标准偏差为4.92%(n=5)。该方法简化和缩短了样品前处理步骤和时间,测定结果与YC/T 346-2010一致,可用于烟草中果胶含量的批量测定。
為瞭提高YC/T 346-2010果膠含量測定方法的分析速度,將標準中醇化除糖、濾渣痠化兩步前處理優化為一步,即痠醇溶液加熱迴流同時除糖和痠化,併將方法改進前後的測定結果進行比較分析。一步前處理方法線性相關繫數為0.9999,迴收率為93.57%~102.29%,測定結果的相對標準偏差為4.92%(n=5)。該方法簡化和縮短瞭樣品前處理步驟和時間,測定結果與YC/T 346-2010一緻,可用于煙草中果膠含量的批量測定。
위료제고YC/T 346-2010과효함량측정방법적분석속도,장표준중순화제당、려사산화량보전처리우화위일보,즉산순용액가열회류동시제당화산화,병장방법개진전후적측정결과진행비교분석。일보전처리방법선성상관계수위0.9999,회수솔위93.57%~102.29%,측정결과적상대표준편차위4.92%(n=5)。해방법간화화축단료양품전처리보취화시간,측정결과여YC/T 346-2010일치,가용우연초중과효함량적비량측정。
The determination method of tobacco pectin in YC/T 346-2010 was improved in order to simplify the analytical procedure. The tobacco sample was directly extracted with acid alcohol solution instead of with alcoholic solution and with acid solution. The method had good linearity with the correlation coefficient of 0.999 9. The recovery of pectin was in the range of 93.57%to 102.29%, and the RSD of the method was 4.92%(n=5). The result of this method had a great agreement with the result of YC/T 346-2010. The method simplified the analytical procedure and was suitable to determine pectin in batch tobacco samples.