广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2014年
11期
126-128
,共3页
吴培慧%孙有娥%郝媛媛%邢海燕%李一辰
吳培慧%孫有娥%郝媛媛%邢海燕%李一辰
오배혜%손유아%학원원%형해연%리일신
蛋制品%微波消解%等离子体原子发射光谱法
蛋製品%微波消解%等離子體原子髮射光譜法
단제품%미파소해%등리자체원자발사광보법
egg products%microwave digestion%plasma atomic emission spectrometry
建立了同时测定蛋制品中铅、锌、铜三种金属元素等离子体原子发射光谱检测方法。样品经微波消解前处理后,处理液进ICP测定。结果显示:3种金属元素的线性范围较宽,相关系数均( r)为0.999以上,检出限分别为0.8、0.4和1.0 mg/kg。该方法稳定可靠、操作简单、试剂消耗量小。
建立瞭同時測定蛋製品中鉛、鋅、銅三種金屬元素等離子體原子髮射光譜檢測方法。樣品經微波消解前處理後,處理液進ICP測定。結果顯示:3種金屬元素的線性範圍較寬,相關繫數均( r)為0.999以上,檢齣限分彆為0.8、0.4和1.0 mg/kg。該方法穩定可靠、操作簡單、試劑消耗量小。
건립료동시측정단제품중연、자、동삼충금속원소등리자체원자발사광보검측방법。양품경미파소해전처리후,처리액진ICP측정。결과현시:3충금속원소적선성범위교관,상관계수균( r)위0.999이상,검출한분별위0.8、0.4화1.0 mg/kg。해방법은정가고、조작간단、시제소모량소。
The plasma atomic emission spectroscopy detection method was developed for the simultaneous determination of lead , zinc and copper three metal elements of egg products.After the sample prior to microwave digestion, handling liquid into the ICP measurement , the results showed that the linear range of the three kinds of metal elements in a wide correlation coefficient (r) of 0.999 or more, the detection limits were 0.8, 0.4 and 1.0 mg/kg, respectively.The method was reliable , simple operation , and small reagent consumption.