华南师范大学学报(自然科学版)
華南師範大學學報(自然科學版)
화남사범대학학보(자연과학판)
JOURNAL OF SOUTH CHINA NORMAL UNIVERSITY (NATURAL SCIENCE EDITION)
2013年
5期
51-54
,共4页
杨震%张璋%黄康荣%周青伟%刘利伟
楊震%張璋%黃康榮%週青偉%劉利偉
양진%장장%황강영%주청위%류리위
金纳米点阵列%AAO模板%热蒸镀%二步氧化法
金納米點陣列%AAO模闆%熱蒸鍍%二步氧化法
금납미점진렬%AAO모판%열증도%이보양화법
Au nanodot arrays%AAO mask%thermal evaporation%two-step anodization
在高真空状态下采用孔径为40 nm的超薄阳极氧化铝( AAO)模板作为掩膜进行金的热蒸镀,制备了平均粒径为35.5 nm、填充密度为1.45×1010 cm-2的金纳米点阵列.探索了高密度有序纳米点阵列的制备工艺.通过扫描电子显微镜(SEM)和原子力显微镜(AFM)对金纳米点阵列进行表面形貌表征,证明超薄AAO模板法明显改善了金纳米点阵列分布的尺寸均匀度和有序度.
在高真空狀態下採用孔徑為40 nm的超薄暘極氧化鋁( AAO)模闆作為掩膜進行金的熱蒸鍍,製備瞭平均粒徑為35.5 nm、填充密度為1.45×1010 cm-2的金納米點陣列.探索瞭高密度有序納米點陣列的製備工藝.通過掃描電子顯微鏡(SEM)和原子力顯微鏡(AFM)對金納米點陣列進行錶麵形貌錶徵,證明超薄AAO模闆法明顯改善瞭金納米點陣列分佈的呎吋均勻度和有序度.
재고진공상태하채용공경위40 nm적초박양겁양화려( AAO)모판작위엄막진행금적열증도,제비료평균립경위35.5 nm、전충밀도위1.45×1010 cm-2적금납미점진렬.탐색료고밀도유서납미점진렬적제비공예.통과소묘전자현미경(SEM)화원자력현미경(AFM)대금납미점진렬진행표면형모표정,증명초박AAO모판법명현개선료금납미점진렬분포적척촌균균도화유서도.
High-density Au nanodot arrays have attracted a lot of interests because of their potential applications in catalyst and biosensor .This article focused on the research of the manufacture of high-density and well-ordered Au nanodot arrays with size of 40 nm ultra-thin Anodic Aluminum Oxide ( AAO) membrane ( the result of our experi-mental exploration ) being the mask .Well-ordered Au nanodot arrays have fabricated by high-vacuum Au thermal e-vaporation with the help of AAO masks bonded on the desired substrates .The diameters of Au nanodots have been highly controlled with 35.5 nm, the packing-density could achieve to as high as 1.45 ×1010 cm-2 .The morphology of the Au nanodot arrays has been investigated by the SEM and AFM .The SEM images confirmed that the uniformi-ty of the size distribution and structural ordering of Au nanodot arrays had been improved by the two -step anodiza-tion of AAO.