CAJ | 학술논문

以模拟氯吡硫磷污染旱田黄土为研究对象，尝试建立相应的氯吡硫磷紫外检测法，并与气相色谱法进行结果对比，采用超声辅助-机械振荡法强化氯吡硫磷提取效果并进行样品实测．研究发现：紫外分光光度法测定氯吡硫磷的标准曲线为 y＝0．0092 x-0．0026，相关系数r为0．9998，紫外法和气相法的精密度、准确度等参数接近．在实验条件下，超声辅助-机械振荡法能显著提高黄土氯吡硫磷的提取效果，回收率为50．20％～61．70％，认为黄土组分（尤其是有机组分）的吸附效应是导致回收率结果偏低的重要因素．紫外分光光度法可以用于旱田黄土氯吡硫磷的检测分析．
이모의록필류린오염한전황토위연구대상，상시건립상응적록필류린자외검측법，병여기상색보법진행결과대비，채용초성보조-궤계진탕법강화록필류린제취효과병진행양품실측．연구발현：자외분광광도법측정록필류린적표준곡선위 y＝0．0092 x-0．0026，상관계수r위0．9998，자외법화기상법적정밀도、준학도등삼수접근．재실험조건하，초성보조-궤계진탕법능현저제고황토록필류린적제취효과，회수솔위50．20％～61．70％，인위황토조분（우기시유궤조분）적흡부효응시도치회수솔결과편저적중요인소．자외분광광도법가이용우한전황토록필류린적검측분석．
The ultraviolet spectrophotometry (UV) was established to reveal the chlorpyrifos concentration ,the results achieved by UV spectrophotometry and gas chromatography (GC) were analyzed ,and the concentration of chlorpyrifos ,extracted from arid loess with ultra-sonic-assisted treatment ,was investigated with UV spectrophotometry .The results showed:the standard curve of chlorpyrifos by UV spectrophotometry is y=0 .009 2 x-0 .002 6 with coefficient of r 0 .999 8 .The experimental parameters of precision and accuracy are similar by UV and GC methods .The ultrasonic-assisted treatment is effective for the extraction process of chlorpyrifos in arid loess (recovery rates vary from 50 .20% to 61 .70% ) ,and the organic components in loess is believed to be an important reason for the low values of recovery rates .The UV spectrophotometry is appropriate for chlorpyrifos analysis in arid loess .