CAJ | 학술논문

分别采用电热板加热、王水浸提和微波消解三种方法对沉积物标准样品中的总汞进行前处理，通过原子荧光光谱仪进行分析测定，试验结果表明，王水浸提法和微波消解法较之电热板加热消解法，消解程度更完全、样品损失量少、操作更简单、测定结果更稳定。
분별채용전열판가열、왕수침제화미파소해삼충방법대침적물표준양품중적총홍진행전처리，통과원자형광광보의진행분석측정，시험결과표명，왕수침제법화미파소해법교지전열판가열소해법，소해정도경완전、양품손실량소、조작경간단、측정결과경은정。
Using electric heating plate,aqua regia extraction and microwave digestion for pretreatment of total hydrargyrum in sediment samples,then,using atomic fluorescence spectrometer for determination. The results shows that,aqua regia extraction and microwave diges-tion have more complete digestion,less loss of sample,more simple and more stable result compared with electric heating plate digestion method.