CAJ | 학술논문

应用超声波技术在温和条件下制得了不同结构的不对称双席夫碱及其配合物。对所制备的样品应用红外、元素分析、电喷雾质谱(ESI-MS)等手段进行了表征，并建立了质谱鉴定方法，得到了目标配体相关的质谱信息。综合各种分析结果证明了席夫碱及其配合物的结构。
응용초성파기술재온화조건하제득료불동결구적불대칭쌍석부감급기배합물。대소제비적양품응용홍외、원소분석、전분무질보(ESI-MS)등수단진행료표정，병건립료질보감정방법，득도료목표배체상관적질보신식。종합각충분석결과증명료석부감급기배합물적결구。
Asymmetric bis-Schiff base and their complexes had been synthesized by ultrasonic technique under mild experimental conditions.The samples were characterized by infrared spectroscopy,element analysis and electrospray mass spectrometry (ESI-MS).The identification method of mass spectrometry was built.The re-sults of element analysis,IR and ESI-MS are consistent with the structure of the target compounds.