染整技术
染整技術
염정기술
TEXTILE DYEING AND FINISHING JOURNAL
2013年
12期
11-14
,共4页
袁久刚%钱伟伟%朱华君%王强%范雪荣%王平%李昭荣
袁久剛%錢偉偉%硃華君%王彊%範雪榮%王平%李昭榮
원구강%전위위%주화군%왕강%범설영%왕평%리소영
超声波%羊毛%碱溶解度%红外%氨基酸分析
超聲波%羊毛%堿溶解度%紅外%氨基痠分析
초성파%양모%감용해도%홍외%안기산분석
ultrasound%wool%alkali solubility%FTIR%amino acids analysis
为了研究超声波处理对羊毛纤维结构的影响,分别测试了处理前后羊毛纤维的碱溶解度、表面组成、结晶度以及处理液氨基酸构成。结果表明:超声波处理对纤维表面及内部结构均有一定的破坏作用,处理后羊毛纤维的损伤程度整体提高。FTIR测试表明,其表面鳞片层中的胱氨酸被进一步氧化成为磺基丙氨酸;XRD测试则显示,纤维结晶指数也有一定程度的降低;而处理液氨基酸分析则表明,超声波处理对纤维的细胞间质也有破坏作用,导致溶液中的高硫蛋白和高酪氨酸蛋白含量增加。
為瞭研究超聲波處理對羊毛纖維結構的影響,分彆測試瞭處理前後羊毛纖維的堿溶解度、錶麵組成、結晶度以及處理液氨基痠構成。結果錶明:超聲波處理對纖維錶麵及內部結構均有一定的破壞作用,處理後羊毛纖維的損傷程度整體提高。FTIR測試錶明,其錶麵鱗片層中的胱氨痠被進一步氧化成為磺基丙氨痠;XRD測試則顯示,纖維結晶指數也有一定程度的降低;而處理液氨基痠分析則錶明,超聲波處理對纖維的細胞間質也有破壞作用,導緻溶液中的高硫蛋白和高酪氨痠蛋白含量增加。
위료연구초성파처리대양모섬유결구적영향,분별측시료처리전후양모섬유적감용해도、표면조성、결정도이급처리액안기산구성。결과표명:초성파처리대섬유표면급내부결구균유일정적파배작용,처리후양모섬유적손상정도정체제고。FTIR측시표명,기표면린편층중적광안산피진일보양화성위광기병안산;XRD측시칙현시,섬유결정지수야유일정정도적강저;이처리액안기산분석칙표명,초성파처리대섬유적세포간질야유파배작용,도치용액중적고류단백화고락안산단백함량증가。
To study the influence of ultrasonic treatment on structure of wool fiber, alkali solubility, functional groups of wool surface, crystallinity and construction of after-treated solution were detailed analyzed. The results showed that ultrasonic treatment ceased some damage to wool fiber. FTIR analysis showed that the cysteine of cuticle layer loaded on wool surface was further oxidized to cysteic acid after the ultrasonic treatment. XRD analysis indicated that the crystal index of wool fiber decreased dramatically. Amino acids analysis of after-treated solution showed that the ultrasonic could also damage the cell membrane cortex, leading to the increase of high sulfur protein and high tyrosine protein content of the solution.