光谱学与光谱分析
光譜學與光譜分析
광보학여광보분석
SPECTROSCOPY AND SPECTRAL ANALYSIS
2014年
1期
221-225
,共5页
郑建平%陆继东%张博%陈世和%姚顺春%潘凤萍%董璇%张曦
鄭建平%陸繼東%張博%陳世和%姚順春%潘鳳萍%董璇%張晞
정건평%륙계동%장박%진세화%요순춘%반봉평%동선%장희
激光能量%煤粉流%激光诱导击穿光谱%等离子体
激光能量%煤粉流%激光誘導擊穿光譜%等離子體
격광능량%매분류%격광유도격천광보%등리자체
Laser energy%Pulverized coal flow%Laser-induced breakdown spectroscopy%Plasma
考察了大气环境下激光诱导击穿光谱适用于煤粉流多元素同时检测的激光能量范围,分析了造成煤粉流测量谱线信号波动的原因,得到了适用于煤粉流多元素同时检测的激发区域功率密度范围和最佳功率密度。实验选取能量范围为20~160mJ,粒径小于200μm煤粉颗粒经下料口自由下落形成煤粉流束,通过螺杆式给粉机控制流量,波长1064nm脉冲激光聚焦后作用于下降的煤粉流束上,产生等离子体,光谱仪采集等离子体发射光谱信号,分析结果表明:实验台架下适于煤粉流LIBS检测的能量范围为30~60mJ,对应激发前沿功率密度选取范围14.4~34.4GW·cm-2,最佳测量功率密度19.5GW·cm-2。
攷察瞭大氣環境下激光誘導擊穿光譜適用于煤粉流多元素同時檢測的激光能量範圍,分析瞭造成煤粉流測量譜線信號波動的原因,得到瞭適用于煤粉流多元素同時檢測的激髮區域功率密度範圍和最佳功率密度。實驗選取能量範圍為20~160mJ,粒徑小于200μm煤粉顆粒經下料口自由下落形成煤粉流束,通過螺桿式給粉機控製流量,波長1064nm脈遲激光聚焦後作用于下降的煤粉流束上,產生等離子體,光譜儀採集等離子體髮射光譜信號,分析結果錶明:實驗檯架下適于煤粉流LIBS檢測的能量範圍為30~60mJ,對應激髮前沿功率密度選取範圍14.4~34.4GW·cm-2,最佳測量功率密度19.5GW·cm-2。
고찰료대기배경하격광유도격천광보괄용우매분류다원소동시검측적격광능량범위,분석료조성매분류측량보선신호파동적원인,득도료괄용우매분류다원소동시검측적격발구역공솔밀도범위화최가공솔밀도。실험선취능량범위위20~160mJ,립경소우200μm매분과립경하료구자유하락형성매분류속,통과라간식급분궤공제류량,파장1064nm맥충격광취초후작용우하강적매분류속상,산생등리자체,광보의채집등리자체발사광보신호,분석결과표명:실험태가하괄우매분류LIBS검측적능량범위위30~60mJ,대응격발전연공솔밀도선취범위14.4~34.4GW·cm-2,최가측량공솔밀도19.5GW·cm-2。
The logical range of laser power density and optimum laser power density were explored for multi-element analysis of pulverized coal flow with laser-induced breakdown spectroscopy in the present paper .The range of laser energy was chosen from 20 to 160 mJ in the experiment .Pulverized coal less than 200 μm in diameter of particles fell freely through feeder outlet and the rate of flow was controlled by screw feeder .Emissions were collected with pulse laser at 1 064 nm focusing on pulverized coal flow and plasma was generated .The intensity and cause of fluctuation of emission spectra at various laser energy levels were studied .A suitable range of laser power density is from 14.4 to 34.4 GW · cm-2 ,and the optimum laser power density is 19.5 GW · cm-2 for the determination of pulverized coal flow with LIBS .