CAJ | 학술논문

以奥克托今炸药（HMX）为高温、高压源，二氧化钛粉末与活性碳粉混合物为主要前驱体，采用爆炸径向冲击法合成了碳化钛粉末。采用扫描电子显微镜（SEM）、X射线衍射（XRD）和差热失重分析仪（DSC-TG）分析了样品的形貌、成分和性能。研究结果表明：样品大小为50nm以内的颗粒，分布性良好，XRD测试数据与理论值吻合较好，且样品在空气气氛下1000℃范围内不易被氧化。
이오극탁금작약（HMX）위고온、고압원，이양화태분말여활성탄분혼합물위주요전구체，채용폭작경향충격법합성료탄화태분말。채용소묘전자현미경（SEM）、X사선연사（XRD）화차열실중분석의（DSC-TG）분석료양품적형모、성분화성능。연구결과표명：양품대소위50nm이내적과립，분포성량호，XRD측시수거여이론치문합교호，차양품재공기기분하1000℃범위내불역피양화。
In this paper, titanium carbide powder was prepared by radial blast shock, high pressure and temperature were created by octogen(HMX) , and titania powder mixture of the active carbon was used as the main precursor. The morphology, composition and performance of the samples were studied by scanning electron microscopy(SEM), X-ray diffraction(XRD) and differential scanning calorimeter-thermo gravimetric analyzer(DSC-TG). The research results show that the particle size of the sample was within 50nm, the distribution of the sample was well. XRD test data were in good agreement with the theoretical value and the sample was difficult to be oxidized in air atmosphere within 1 000℃.