黑龙江医药
黑龍江醫藥
흑룡강의약
HEILONGJIANG MEDICAL JOURNAL
2013年
6期
988-990,991
,共4页
刘跃喜%张文丽%王德
劉躍喜%張文麗%王德
류약희%장문려%왕덕
脉通口服液%薄层色谱%高效液相色谱%葛根素,原儿茶醛
脈通口服液%薄層色譜%高效液相色譜%葛根素,原兒茶醛
맥통구복액%박층색보%고효액상색보%갈근소,원인다철
Mai Tong OralLiquid%TCL%HPLC%Puerarin%Protocatechuicaldehude
目的：制定脉通口服液（葛根，丹参）的质量标准。方法：用TCL鉴别制剂中葛根、丹参；采用HPLC法测定葛根素的含量。结果：TLC色谱中均能明显的检出葛根、丹参；HPLC法测得葛根素含量2.2920mg/ml，平均回收率为99.14％，RSD为1.51％（n=5）。定性、定量方法简便，准确，专属性强。结论：建立的方法能有效地控制脉通口服液的质量。
目的：製定脈通口服液（葛根，丹參）的質量標準。方法：用TCL鑒彆製劑中葛根、丹參；採用HPLC法測定葛根素的含量。結果：TLC色譜中均能明顯的檢齣葛根、丹參；HPLC法測得葛根素含量2.2920mg/ml，平均迴收率為99.14％，RSD為1.51％（n=5）。定性、定量方法簡便，準確，專屬性彊。結論：建立的方法能有效地控製脈通口服液的質量。
목적：제정맥통구복액（갈근，단삼）적질량표준。방법：용TCL감별제제중갈근、단삼；채용HPLC법측정갈근소적함량。결과：TLC색보중균능명현적검출갈근、단삼；HPLC법측득갈근소함량2.2920mg/ml，평균회수솔위99.14％，RSD위1.51％（n=5）。정성、정량방법간편，준학，전속성강。결론：건립적방법능유효지공제맥통구복액적질량。
Objective:To establish the method for quality control of Mai Tong Oral Liquid (Pueerarin;Protocatechuicaldehude). Meth-ods;Puerarin;Protocatechuicaldehude in this medicine were identified by TCL.The content of Puerarin in this medicine was determined by HPLC.Results;Puerarin;Protocatechuicaldehude could be identified by TCL.The content of Puerarin was determined by HPLC was 2.2920mg/ml.The average recovery was99.14%and RSD was 1.51%(n=5).Conclusion:The method was simple,accurate and with strong specificity and can be used for the quality control of Mai Tong Oral Liquid.
