国际医药卫生导报
國際醫藥衛生導報
국제의약위생도보
INTERNATIONAL MEDICINE & HEALTH GUIDANCE NEWS
2009年
19期
78-80
,共3页
复方祛风止痛外用颗粒%丁香%威灵仙%桂枝%薄层色谱法%定性鉴别
複方祛風止痛外用顆粒%丁香%威靈仙%桂枝%薄層色譜法%定性鑒彆
복방거풍지통외용과립%정향%위령선%계지%박층색보법%정성감별
Qufeng topical analgesic compound particles%Flos Caryophyllata%Radix Clematidis%Ramulus Cinnamomi%TLC%Qualitative identification
目的 建立复方祛风止痛外用颗粒中主要成分的薄层色谱鉴别方法,为研究该复方制剂的质量标准奠定基础.方法采用薄层色谱分析方法对该制剂中的丁香、威灵仙、桂枝等药材进行定性鉴别.结果各供试品色谱中,在与各自对照品色谱相同的位置上,显相同颜色的斑点,阴性对照无干扰.结论该鉴别方法专属性强、重现性好、灵敏度高,可作为该复方制剂的质量控制方法之一.
目的 建立複方祛風止痛外用顆粒中主要成分的薄層色譜鑒彆方法,為研究該複方製劑的質量標準奠定基礎.方法採用薄層色譜分析方法對該製劑中的丁香、威靈仙、桂枝等藥材進行定性鑒彆.結果各供試品色譜中,在與各自對照品色譜相同的位置上,顯相同顏色的斑點,陰性對照無榦擾.結論該鑒彆方法專屬性彊、重現性好、靈敏度高,可作為該複方製劑的質量控製方法之一.
목적 건립복방거풍지통외용과립중주요성분적박층색보감별방법,위연구해복방제제적질량표준전정기출.방법채용박층색보분석방법대해제제중적정향、위령선、계지등약재진행정성감별.결과각공시품색보중,재여각자대조품색보상동적위치상,현상동안색적반점,음성대조무간우.결론해감별방법전속성강、중현성호、령민도고,가작위해복방제제적질량공제방법지일.
Objective To set up the thin-layer ehromatogram method of the principal in-gredients in Gufeng topical analgesic compound particles,and to establish the foundation for the quality control standar.Methods The TCL method was adopted to distinguish the Flos Caryophyllata;Radix Clematidis.Ramulus Cinnamomi in this drug.Results The characteristic spots on the chromatogram of the preparation were corresponding to the ones of contrast product,and the negative contrast had on disturbance.Conclusions This method has the good of specialization,reproducibility,and sensitivity.It can be used for the quality control of Qufeng topical analgesic compound particles.
