CAJ | 학술논문

采用高效液相色谱法，以甲醇＋水为流动相(体积比50∶50，pH值8.5)，流速为0.8 mL/min，使用Agilent TC-C 18(2)反相色谱柱与紫外可变波长检测器，在250 nm波长下用外标法对福美锌原药进行分离和定量分析。结果表明：该方法的线性相关系数为0.9997，标准偏差为0.18，变异系数为0.19%，平均回收率为99.4%。
채용고효액상색보법，이갑순＋수위류동상(체적비50∶50，pH치8.5)，류속위0.8 mL/min，사용Agilent TC-C 18(2)반상색보주여자외가변파장검측기，재250 nm파장하용외표법대복미자원약진행분리화정량분석。결과표명：해방법적선성상관계수위0.9997，표준편차위0.18，변이계수위0.19%，평균회수솔위99.4%。
A method for separation and quantitative analysis of ziram TC was established by HPLC using methanol and water (volume ratio of 50︰50, pH 8.5) as mobile phase with a flow rate of 0.8 mL/min, Agilent TC-C 18 (2) column and a variable wavelength UV detector at 250 nm. The results showed that the linear correlation coefficient was 0.999 7, the standard deviation was 0.18, the variation coefficient was 0.19%, and the average recovery was 99.4%.