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万方数据

食品研究与开发 식품연구여개발
FOOD RESEARCH AND CEVELOPMENT
2013年 23期 41-44 ,共4页

于杰%李晓玉%李淑娟%李淼%董丽萍%高群%高玉生%隋涛

우걸%리효옥%리숙연%리묘%동려평%고군%고옥생%수도

基质效应%氨基甲酸酯类农药%高效液相色谱-串联质谱法基質效應%氨基甲痠酯類農藥%高效液相色譜-串聯質譜法
기질효응%안기갑산지류농약%고효액상색보-천련질보법
matrix effect%carbamate pesticide residues%high performance liquid chromatography-tandem mass spectrometry

通过提取后添加法定量分析了13种氨基甲酸酯类农药在高效液相色谱-串联质谱检测中的基质效应。得到13种氨基甲酸酯类农药在不同浓度的基质中基质效应因子，对基质效应受到化合物性质、基质种类、基质浓度等因素的影响进行了评价。
통과제취후첨가법정량분석료13충안기갑산지류농약재고효액상색보-천련질보검측중적기질효응。득도13충안기갑산지류농약재불동농도적기질중기질효응인자，대기질효응수도화합물성질、기질충류、기질농도등인소적영향진행료평개。
Quantitative analysis the matrix effects of 13 carbamate pesticides using high performance liquid chromatography-tandem mass spectrometry by post-extraction spiking method. The matrix effect factors of 13 carbamate pesticides were found from different concentrations of different samples. It was found that compound charactors, sample types and concentration had affected the matrix effects.