CAJ | 학술논문

以邻苯二酚为原料经环化、缩合、氧化脱羧反应制得洋茉莉醛并表征了其结构，其中在氧化脱羧阶段，使用了自制的新型高效过氧化物/金属盐复合催化剂，优化后的工艺总收率为84.8%。此工艺与已有文献报道相比，具有原料易得、工艺简单、反应迅速、产率高等优势，有良好的工业化前景。
이린분이분위원료경배화、축합、양화탈최반응제득양말리철병표정료기결구，기중재양화탈최계단，사용료자제적신형고효과양화물/금속염복합최화제，우화후적공예총수솔위84.8%。차공예여이유문헌보도상비，구유원료역득、공예간단、반응신속、산솔고등우세，유량호적공업화전경。
Catechol was used as the raw material , and the heliotropine was reached by cyclization reaction , condensation reaction and oxidative decarboxylation reaction , with a total yield of 84.8%. Its structure was also characterized. In the oxidative decarboxylation reaction , a new catalyzer was used. Compared with the exiting literature, this technology is easily obtained raw material, simple process, high yield and good industrial prospects.